Zobrazeno 1 - 10
of 88
pro vyhledávání: '"Shoji Takitani"'
Publikováno v:
Analytical Sciences. 11:405-409
An electrochemical method has been developed for the determination of L-ascorbic acid (AsA) by a flow injection analysis. The method is based on a reaction of AsA with copper(II) at pH 5.0 to form a readily oxidizable species, followed by electrochem
Publikováno v:
Biomedical Chromatography. 8:184-188
Carbonic anhydrase (CA)-immobilized aminopropyl silica precolumn was developed for direct injection determination of certain sulphonamide drugs in biological fluids by column-switching (CS) high-performance liquid chromatography. Under the optimized
Publikováno v:
Journal of Liquid Chromatography. 17:1281-1290
The disadvantage of anhydrotrypsin-immobilized diol silica column, retention of basic peptides having no Arg or Lys at their C-termini and no retention of certain C-termina! Arg peptide, was overcome by using 10 mM acetate buffer (pH 6.0) containing
Publikováno v:
Chemosphere. 27:2155-2162
Aqueous benz(a)anthracene [B(a)A] solution was treated with chlorine in the absence and presence of bromide ion. Changes in the composition of the halogenated products in water were determined by high performance liquid chromatographic (HPLC) analyse
Publikováno v:
Journal of Chromatography A. 637:35-41
A column switching high-performance liquid chromatographic system in which peptides retained on an anhydrochymotrypsin (AHC)-immobilized diol-silica precolumn were selectively transferred to and separated on a reversed-phase analytical column was dev
Publikováno v:
Chromatographia. 35:321-324
A simple and sensitive ion chromatographic method for the estimation of tresyl groups on several activated supports (tresylated diol silica, tresylated Sepharose 4B and Tresyl-5PW) has been developed. The method involves the hydrolysis of tresyl grou
Publikováno v:
Journal of Environmental Chemistry. 3:561-569
Studies were performed to develop a simple and sensitive method for detection of mutagens in water. The proposed method consists of solid phase extraction using Sep-Pak-tC18 cartridge and mutagenicity test of the cartridge extracts by the microsuspen
Publikováno v:
Fresenius' Journal of Analytical Chemistry. 345:63-67
A HPLC method using a fluorescence detector is described for the determination of halogenated benz(a)anthracenes (BAX, x=Cl or Br) in water. It consists of the following three procedures; (1) liquid-liquid extraction of BAX with benzene, (2) eliminat
Publikováno v:
Journal of Chromatography B: Biomedical Sciences and Applications. 582:131-135
A method for the determination of cyanide in human red cells has been developed. Cyanide was extracted from red cells by adding water and methanol, and then derivatized with 2,3-naphthalene-dialdehyde and taurine to give a fluorescent product, which
Publikováno v:
Chromatographia. 33:113-116
Anhydrochymotrypsin (AHC), a catalytically inert derivative of chymotrypsin in which the serine-residue active site has been converted chemically to a dehydroalanine residue, was immobilized on diol silica by activation with trifluoroethanesulfonyl c