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A solvent-free synthesis of (thio)ester derivatives using FeCl3 as a heterogeneous catalyst

Publikováno v: Tetrahedron Letters. 123

A simple, solvent-free method for the synthesis of (thio)esters from simple acid chlorides at room temperature is reported. Simple FeCl3 (5 mol%) enables facile, near complete conversion of equimolar starting materials in high selectivity. Recycling

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Akademický článek

A solvent-free synthesis of (thio)ester derivatives using FeCl3 as a heterogeneous catalyst

Autor: Younes, Sabry H.H., Hollmann, F.

Publikováno v: In Tetrahedron Letters 23 June 2023 123

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Akademický článek

Structure of the Reductase Domain of a Fungal Carboxylic Acid Reductase and Its Substrate Scope in Thioester and Aldehyde Reduction.

Autor: Daniel, Bastian, Hashem, Chiam, Leithold, Marlene, Sagmeister, Theo, Tripp, Adrian, Stolterfoht-Stock, Holly, Messenlehner, Julia, Keegan, Ronan, Winkler, Christoph K., Ling, Jonathan Guyang, Younes, Sabry H.H., Oberdorfer, Gustav, Abu Bakar, Farah Diba, Gruber, Karl, Pavkov-Keller, Tea, Winkler, Margit

Publikováno v: ACS Catalysis; 5/5/2023, Vol. 13 Issue 9, p15668-15674, 7p

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Structure of the Reductase Domain of a Fungal Carboxylic Acid Reductase and Its Substrate Scope in Thioester and Aldehyde Reduction

Autor: Bastian Daniel, Chiam Hashem, Marlene Leithold, Theo Sagmeister, Adrian Tripp, Holly Stolterfoht-Stock, Julia Messenlehner, Ronan Keegan, Christoph K. Winkler, Jonathan Guyang Ling, Sabry H.H. Younes, Gustav Oberdorfer, Farah Diba Abu Bakar, Karl Gruber, Tea Pavkov-Keller, Margit Winkler

Publikováno v: ACS Catalysis, 12(24)

The synthesis of aldehydes from carboxylic acids has long been a challenge in chemistry. In contrast to the harsh chemically driven reduction, enzymes such as carboxylic acid reductases (CARs) are considered appealing biocatalysts for aldehyde produc

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