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pro vyhledávání: '"SHELTON BANK"'
Autor:
Shelton Bank
Publikováno v:
Concepts in Magnetic Resonance. 9:83-93
Nuclear magnetic resonance spectroscopy often uses complex methodologies in complex applications. In this review, some of the details of NMR spectroscopy are made more accessible and more interesting. Determinations of components of everyday interest
Publikováno v:
Canadian Journal of Microbiology. 42:1219-1224
The gram-negative anaerobe Oxalobacter formigenes, grows on oxalate as the principal carbon and energy source, but a small amount of acetate is also required for growth. Experiments were conducted to determine the distribution and the position of lab
Solid 13C CPMAS NMR spectroscopy studies of biosynthesis in whole cells of Methanosphaera stadtmanae
Publikováno v:
Solid State Nuclear Magnetic Resonance. 7:253-261
Whole cells of Methanosphaera stadtmanae were grown in media containing [13C]CO2, [2-13C]acetate, [1-13C]acetate, [3-13C]serine and [1-13C]formate. The label incorporation was determined using solid state 13C CPMAS NMR spectroscopy. The incorporation
Publikováno v:
Chemico-Biological Interactions. 102:101-116
The Paal-Knorr condensation reaction between the γ-diketone 2,5-hexanedione (2,5-HD) and e-amine moieties of proteins of various molecular weight, including ribonuclease (RNase), bovine serum albumin (BSA) and rat neurofilament (NF), has been invest
Publikováno v:
Chemical Research in Toxicology. 8:764-771
n-Hexane is metabolized to the gamma-diketone 2,5-hexanedione (2,5-HD), a derivative that covalently binds to lysine residues in neurofilament (NF) protein to yield 2,5-dimethylpyrrole adducts. Studies comparing the pyrrole-forming potential and neur
Publikováno v:
Applied and Environmental Microbiology. 61:1180-1186
We found that general pathways for amino acid synthesis of Methanosphaera stadtmanae, a methanogen that forms CH(inf4) from H(inf2) and methanol, resembled those of methanogens that form CH(inf4) from CO(inf2) or from the methyl group of acetate. We
Publikováno v:
Chemical Research in Toxicology. 7:551-558
2,5-Hexanedione (2,5-HD) is the neurotoxic gamma-diketone metabolite of the industrial solvent n-hexane. Substantial evidence indicates that 2,5-HD reacts with neurofilament protein lysine epsilon-amines to yield 2,5-dimethylpyrrole adducts and that
Publikováno v:
Langmuir. 10:1528-1531
The cross-polarization magic angle spinning (CPMAS) NMR spectra of I5N-enriched 2-phenethylamine as the ammonium salt and adsorbed on an aluminum-exchanged clay are compared with spectra for natural abundance 2-phenethylamine. An important gain in re
Publikováno v:
Clays and Clay Minerals. 41:95-102
Phenethylamine ~3C_enriched in the beta position was adsorbed on four different aluminum- exchanged days: hectorite, Barasym, Laponite RD, and lithium taeniolite. The sites for adsorption were characterized by ~3C high-resolution cross-polarization m
Autor:
Shelton Bank
Publikováno v:
ChemInform. 28
Nuclear magnetic resonance spectroscopy often uses complex methodologies in complex applications. In this review, some of the details of NMR spectroscopy are made more accessible and more interesting. Determinations of components of everyday interest