Zobrazeno 1 - 10
of 64
pro vyhledávání: '"S. Grzejszczak"'
Autor:
Michał W. Wieczorek, Marian Mikołajczyk, Fernando Montanari, Wanda H. Midura, S. Grzejszczak, Mauro Cinquini, Janina Karolak-Wojciechowska
Publikováno v:
Tetrahedron. 50:8053-8072
Chlorination of α-phosphoryl sulfoxides 1 with iodobenzene dichloride and sulfuryl chloride in the presence and in the absence of pyridine and stereochemical investigations of this reaction using (+)-(S)-α-dimethoxyphosphorylmethyl p-tolyl sulfoxid
Autor:
S. Grzejszczak, Fernando Montanari, Mauro Cinquini, Marian Mikołajczyk, Wanda H. Midura, Janina Karolak-Wojciechowska, Michał W. Wieczorek
Publikováno v:
ChemInform. 25
Publikováno v:
Tetrahedron. 35:1019-1025
Additive increments for para and meta substituents in the aromatic ring were calculated on the basis of 332 examples of chemical shifts and were correlated with Hammett's constants. Examples of calculation of chemical shifts of olefinic protons in su
Publikováno v:
Phosphorus and Sulfur and the Related Elements. 10:369-373
A convenient method is described for the formation of distyryl sulphides, sulphoxides and sulphones. Thus, Horner-Wittig reaction in two-phase system of the corresponding phosphonates with aromatic aldehydes affords the desired α β unsaturated sulp
Publikováno v:
Tetrahedron Letters. 17:477-480
Autor:
Burkhard Costisella, S. Grzejszczak, B. Mlotkowska, Hans Gross, Marian Mikołajczyk, Andrzej Zatorski
Publikováno v:
Tetrahedron. 34:3081-3088
A new and general synthesis of ketene S,S-thioacetals (1) and ketene O.S-thioacetals (6) which involves the Horner-Wittig reaction of carbonyl compounds with the metallated S,S- and O,S-thioacetals of formyl-phosphonates (4 and 5) is described. The H
Publikováno v:
The Journal of Organic Chemistry. 43:2518-2521
Publikováno v:
Tetrahedron Letters. 23:2237-2240
An effective synthesis of 1,4-dicarbonyl systems involving the Horner—Wittig reaction of α-phosphoryl sulphides with the half-protected 1,3-dicarbonyl compounds followed by hydrolysis of the vinyl sulphides formed is described. The total synthesis
Publikováno v:
Tetrahedron Letters. 25:2489-2492
Oxidation of the α-alkylthio-substituted phosphonate carbanions was found to give the corresponding carbonyl compounds. A new synthesis of 1,4-dicarbonyl systems involving the oxygenation of phosphonate carbanions as a key step is described. Total s
Autor:
S. Grzejszczak, Burkhard Costisella, B. Mlotkowska, A. Zatorski, Hans Gross, Marian Mikołajczyk
Publikováno v:
Journal f�r Praktische Chemie. 319:17-22
Die Synthese von offenkettigen und cyclischen Alkyl- bzw. Aryl-S,S-acetalen von Formylphosphonsaureestern nach verschiedenen Methoden wird beschrieben. Die 1H-, 13C- und 31P-NMR-Spektren dieser Verbindungen werden diskutiert. α-Substituted Phosphona