Zobrazeno 1 - 10
of 10
pro vyhledávání: '"Rosella M. O'Mahony"'
Publikováno v:
Organic Process Research & Development
Generation of tosyl azide 12 in acetonitrile in flow under water-free conditions using an azide resin and its use in diazo transfer to a series of aryl acetates are described. Successful telescoping with a rhodium acetate-catalyzed O–H insertion ha
Autor:
Denis Lynch, Lorraine M. Bateman, Daniel G. McCarthy, Rosella M. O'Mahony, Stuart G. Collins, Anita R. Maguire
Publikováno v:
European Journal of Organic Chemistry. 2019:3575-3580
Publikováno v:
Tetrahedron Letters. 60:35-39
Herein, we report the preparation and use of m-carboxybenzenesulfonyl azide as a diazo transfer reagent. This compound is an inexpensive and potentially scalable alternative to many of the diazo transfer reagents currently available, most of which ha
Autor:
Rosella M. O'Mahony, Stuart G. Collins, Brian Glennon, Roderick C. Jones, Philip Donnellan, Anita R. Maguire, Denis Lynch, Eilís Ní Thuama, Hannah L. D. Hayes
Publikováno v:
European Journal of Organic Chemistry. 2017:6533-6539
The hazardous diazo transfer reagent mesyl azide, has been safely generated and used in situ for continuous diazo transfer as part of an integrated synthetic process with an embedded safety quench. Diazo transfer to β-ketoesters and a β-ketosulfone
Autor:
Benjamin J. Deadman, Rosella M. O'Mahony, Stuart G. Collins, Daniel C. Crowley, Denis Lynch, Anita R. Maguire
Publikováno v:
Organic & Biomolecular Chemistry. 14:3423-3431
Heat and shock sensitive tosyl azide was generated and used on demand in a telescoped diazo transfer process. Small quantities of tosyl azide were accessed in a 'one pot' batch procedure using shelf stable, readily available reagents. For large scale
Publikováno v:
Tetrahedron Letters. 60:1311
Autor:
Lynch, Denis1 (AUTHOR), O'Mahony, Rosella M.1 (AUTHOR), McCarthy, Daniel G.1 (AUTHOR), Bateman, Lorraine M.2 (AUTHOR), Collins, Stuart G.1 (AUTHOR) stuart.collins@ucc.ie, Maguire, Anita R.2 (AUTHOR) a.maguire@ucc.ie
Publikováno v:
European Journal of Organic Chemistry. 6/16/2019, Vol. 2019 Issue 22, p3575-3580. 6p.
Autor:
O'Mahony, Rosella M.1, Lynch, Denis1, Hayes, Hannah L. D.1, Ní Thuama, Eilís1, Donnellan, Philip2, Jones, Roderick C.2, Glennon, Brian2, Collins, Stuart G.1 stuart.collins@ucc.ie, Maguire, Anita R.3 a.maguire@ucc.ie
Publikováno v:
European Journal of Organic Chemistry. Dec2017, Vol. 2017 Issue 44, p6533-6539. 7p.
Publikováno v:
Organic & Biomolecular Chemistry; 4/7/2016, Vol. 14 Issue 13, p3339-3344, 6p
Autor:
Deadman, Benjamin J., O'Mahony, Rosella M., Lynch, Denis, Crowley, Daniel C., Collins, Stuart G., Maguire, Anita R.
Publikováno v:
Organic & Biomolecular Chemistry; 4/7/2016, Vol. 14 Issue 13, p3423-3431, 9p