Zobrazeno 1 - 10
of 159
pro vyhledávání: '"Robert W. Schurko"'
Autor:
Louae M. Abdulla, Austin A. Peach, Sean T. Holmes, Zachary T. Dowdell, Lara K. Watanabe, Emilia M. Iacobelli, David A. Hirsh, Jeremy M. Rawson, Robert W. Schurko
Publikováno v:
Crystal Growth & Design. 23:3412-3426
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::03cbc239dfa2b4470af0203fba236aa8
https://doi.org/10.1021/acs.cgd.2c01539
https://doi.org/10.1021/acs.cgd.2c01539
Publikováno v:
CrystEngComm. 25:213-224
Competitive and stability milling reactions, along with 35Cl solid-state NMR and powder X-ray diffraction measurements, are used to assess coformer affinity and cocrystal stability for a series of fluoxetine HCl cocrystals.
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::d1279d14599b70b2ca784b50e461ce2b
https://doi.org/10.1039/d2ce01341j
https://doi.org/10.1039/d2ce01341j
Publikováno v:
CrystEngComm. 24:2626-2641
This work discusses the mechanochemical synthesis and characterization of five urea multicomponent crystals by XRD, solid-state NMR, DFT and ab initio molecular dynamics calculations to provide insights into their molecular-level structures.
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::517a5b6fabde99f239b6fccb05522f55
https://doi.org/10.1039/d1ce01610e
https://doi.org/10.1039/d1ce01610e
Publikováno v:
Molecular Pharmaceutics. 19:440-455
This study uses 35Cl and 14N solid-state NMR (SSNMR) spectroscopy and dispersion-corrected plane-wave density functional theory (DFT) calculations for the structural characterization of chloride salts of nutraceuticals in their bulk and dosage forms.
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::63c59ba989c3b7487764bb4454720283
https://doi.org/10.1021/acs.molpharmaceut.1c00708
https://doi.org/10.1021/acs.molpharmaceut.1c00708
Publikováno v:
Journal of the American Chemical Society
Chemical exchange saturation transfer (CEST) enhances solution-state NMR signals of labile and otherwise invisible chemical sites, by indirectly detecting their signatures as a highly magnified saturation of an abundant resonance─for instance, the
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_dedup___::6f34cb5e6968e3eae0a843f372717150
http://europepmc.org/articles/PMC8640991
http://europepmc.org/articles/PMC8640991
3D relaxation-assisted separation of wideline solid-state NMR patterns for achieving site resolution
Publikováno v:
Physical chemistry chemical physics : PCCP. 24(37)
There are currently no methods for the acquisition of ultra-wideline (UW) solid-state NMR spectra under static conditions that enable reliable separation and resolution of overlapping powder patterns arising from magnetically distinct nuclei. This st
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_dedup___::04271667eb937fd3ff61d56a55c0934f
https://pubmed.ncbi.nlm.nih.gov/36112060
https://pubmed.ncbi.nlm.nih.gov/36112060
Publikováno v:
Magnetic Resonance in Chemistry. 59:1009-1023
Solid-state NMR (SSNMR) spectroscopy of integer-spin quadrupolar nuclei is important for the molecular-level characterization of a variety of materials and biological solids; of the integer spins, 2 H (S = 1) is by far the most widely studied, due to
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_dedup___::d40e56097c62040ef6825473c73f5786
https://doi.org/10.1002/mrc.5145
https://doi.org/10.1002/mrc.5145
Autor:
Robert W. Schurko, Stephen J. Loeb, Cameron S. Vojvodin, Benjamin H. Wilson, Ghazale Gholami, Louae M. Abdulla, Christopher A. O’Keefe
Publikováno v:
Chem. 7:202-211
Summary An H-shaped [2]rotaxane with a biphenyl axle and a 24-crown-8 (24C8) macrocycle was inserted into the tetrahedral cavities of the isostructural fcu MOFs PCN-57, UiO-68-d4, and UWCM-10. The resulting rotaxane containing MOFs UWDM-8, UWDM-9-d4,
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::bc3e746b92cdb285e8436f86699faf1f
https://doi.org/10.1016/j.chempr.2020.11.009
https://doi.org/10.1016/j.chempr.2020.11.009
Autor:
Benjamin H. Wilson, Kelong Zhu, Robert W. Schurko, Ghazale Gholami, Christopher A. O’Keefe, Stephen J. Loeb
Publikováno v:
Faraday Discussions. 225:358-370
Zr(iv) metal-organic frameworks (MOFs) UiO-68 and PCN-57, containing triphenylene dicarboxylate (TPDC) and tetramethyl-triphenylene dicarboxylate (TTDC) linkers, respectively, were doped with an H-shaped tetracarboxylate linker that contains a [2]rot
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_dedup___::ee22394ce5700d2a1e5487c8f891adcf
https://doi.org/10.1039/d0fd00004c
https://doi.org/10.1039/d0fd00004c
Publikováno v:
Chemical Science
A new [2]rotaxane molecular shuttle linker based on the binding of a 24-crown-8 ether macrocycle at a benzimidazole recognition site was synthesised. The shuttling dynamics of the linker were studied in solution and the structure confirmed by X-ray c
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_dedup___::fcae37e646fa505abd36646c90806e6f
https://doi.org/10.1039/d0sc06837c
https://doi.org/10.1039/d0sc06837c