Zobrazeno 1 - 10 of 79 pro vyhledávání: '"Robert M. Giuliano"'
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Akademický článek
Allyl 3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-d-glucopyranoside
Autor: Hannah Curran, Chenyao Zhang, Nicholas A. Piro, W. Scott Kassel, Robert M. Giuliano
Publikováno v: IUCrData, Vol 1, Iss 8, p x161363 (2016)
The protected glycoside of 2-amino-2-deoxyglucose (glucosamine), namely allyl 3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-d-glucopyranoside, C23H25NO10, was synthesized from the glycosyl bromide. Crystallographic analysis confirmed the β-anomeric co
Externí odkaz: https://doaj.org/article/bee0822c7f2347a19fdfb5635125516f
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2
Synthesis of Pyranopyrans Related to Diplopyrone and Evaluation as Antibacterials and Herbicides
Autor: Jack H. Roireau, Nicholas C. Lazzara, Dennis D. Wykoff, Robert M. Giuliano, Stephen O. Duke, Thomas Chen, Kevin K. Schrader, Joanna Bajsa-Hirschel, Robert J. Rosano
Publikováno v: Journal of Agricultural and Food Chemistry. 68:9906-9916
Stereoselective syntheses of new pyranopyrans that are related to the natural product diplopyrone, which is a phytotoxin implicated in cork oak decline, have been achieved from carbohydrate starting materials in two approaches that are based on
Externí odkaz: https://explore.openaire.eu/search/publication?articleId=doi_dedup___::a090c19860d9653dde5d658cd4dc0592
https://doi.org/10.1021/acs.jafc.0c02564
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3
Synthesis and crystal structure of (2S,4aR,8aR)-6-oxo-2,4a,6,8a-tetrahydropyrano[3,2-b]pyran-2-carboxamide
Autor: Jack H. Roireau, Scott Kassel, Robert M. Giuliano, Michael W. Giuliano, Mark W. Bezpalko, John Greene, Noa Kopplin
Publikováno v: Acta Crystallographica Section E: Crystallographic Communications, Vol 76, Iss 5, Pp 761-764 (2020)
Acta Crystallographica Section E: Crystallographic Communications
(2S,4aR,8aR)-6-Oxo-2,4a,6,8a-tetra­hydro­pyrano[3,2-b]pyran-2-carboxamide, a potentially effective anti­bacterial agent, was prepared by a chemoselective hydration of the corresponding nitrile using a heterogeneous catalytic method based on copper
Externí odkaz: https://explore.openaire.eu/search/publication?articleId=doi_dedup___::934667ecd92874c3d663d05f308a1402
https://doi.org/10.1107/s2056989020001292
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4
Synthesis and Biological Evaluation of 6-[(1R)-1-Hydroxyethyl]-2,4a(R),6(S),8a(R)-tetrahydropyrano-[3,2-b]-pyran-2-one and Structural Analogues of the Putative Structure of Diplopyrone
Autor: Deanna L. Zubris, Wm Scott Kassel, Robert J. Rosano, Robert M. Giuliano, Stephen O. Duke, Walter J. Boyko, David E. Wedge, Matthew Giovine, Mark W. Bezpalko, Purav P. Vagadia, Kevin K. Schrader, Nicholas A. Piro, Nicholas C. Lazzara
Publikováno v: The Journal of Organic Chemistry. 84:666-678
The phytotoxin diplopyrone is considered to be the main phytotoxin in a fungus that is responsible for cork oak decline. A carbohydrate-based synthesis of the enantiomer of the structure proposed for diplopyrone has been developed from a commercially
Externí odkaz: https://explore.openaire.eu/search/publication?articleId=doi_dedup___::72519aba8a25c79cd0021a321594d764
https://doi.org/10.1021/acs.joc.8b02490
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5
Synthesis of 4-Amino-4-Deoxy Sugar Components of Antibiotics and Bacterial Glycans
Autor: Robert M. Giuliano
The synthesis of 4-amino-4-deoxy carbohydrates that occur in antibiotics and in bacterial glycans is described. The focus of the coverage is on literature published since 2000; however, earlier work is included in some cases for the purposes of histo
Externí odkaz: https://explore.openaire.eu/search/publication?articleId=doi_________::157fd6706c4824111d2c9b4426dcfabe
https://doi.org/10.1016/b978-0-12-409547-2.12710-6
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6
Synthesis and x-ray crystallographic analysis of 4,6-di-O-acetyl-2,3-dideoxy-α-d-threo-hexopyranosyl cyanide
Autor: Scott Kassel, William G. Dougherty, Walter J. Boyko, Madeline E. Rotella, Robert M. Giuliano, Matthew Giovine
Publikováno v: Carbohydrate Research. 425:40-42
The glycopyranosyl cyanide 4,6-di-O-acetyl-2,3-dideoxy-α-D-threo-hexopyranosyl cyanide has been synthesized from tri-O-acetyl-D-galactal by reaction with trimethylsilyl cyanide in the presence of boron trifluoride diethyl etherate followed by cataly
Externí odkaz: https://explore.openaire.eu/search/publication?articleId=doi_dedup___::3a059665cfe79c42d029f157cff972bf
https://doi.org/10.1016/j.carres.2016.03.001
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9
Allyl 3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranoside
Autor: C. Zhang, Robert M. Giuliano, W.S. Kassel, Nicholas A. Piro, H. Curran
Publikováno v: IUCrData, Vol 1, Iss 8, p x161363 (2016)
The protected glycoside of 2-amino-2-deoxyglucose (glucosamine), namely allyl 3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranoside, C23H25NO10, was synthesized from the glycosyl bromide. Crystallographic analysis confirmed the β-anomeric co
Externí odkaz: https://explore.openaire.eu/search/publication?articleId=doi_dedup___::04581d691a3b9ea09e45bb58c04a2f62
https://doi.org/10.1107/s2414314616013638
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10
Synthesis of cyclopropyl glycosides and their use as novel glycosyl donors
Autor: Robert M. Giuliano, Johnson David A, Christopher Cummings, Walter J. Boyko, Clark Scholl, Thomas Licisyn, Kevin L. Hughes
Publikováno v: Carbohydrate Research. 356:288-294
Methods for the synthesis of cyclopropyl glycosides and their use as glycosyl donors are described. Cyclopropyl glycosides containing different substituents were prepared by cyclopropanation of the corresponding vinyl glycosides, or by glycosidation
Externí odkaz: https://explore.openaire.eu/search/publication?articleId=doi_dedup___::d977cfb9cd41de577326e4fe431b2eeb
https://doi.org/10.1016/j.carres.2012.03.008
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