Zobrazeno 1 - 10
of 34
pro vyhledávání: '"Robert C. Mebane"'
Autor:
Robert C. Mebane, Thomas R. Rybolt
Publikováno v:
Journal of Chemical Education. 95:1402-1405
A low-cost alternative to the typical scientific laboratory water bath or a hot plate stirrer water bath is proposed. Readily available immersion circulators have been developed for sous vide cooking. These precision cookers are designed to maintain
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::a73dde2c4028824a9e18eb3f21c55b09
https://doi.org/10.1021/acs.jchemed.8b00163
https://doi.org/10.1021/acs.jchemed.8b00163
Autor:
Daniel R. Zuidema, Robert C. Mebane, Karin J. Bosma, Katherine J. Wert, Abigail L. Smith, Sarah L. Williams
Publikováno v:
Synthetic Communications. 41:2927-2931
Aryl ketones are readily deoxygenated to their corresponding aryl alkanes upon treatment with Raney nickel catalyst in boiling 2-propanol.
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::486a085c67ce34087880696b23d28e25
https://doi.org/10.1080/00397911.2010.515367
https://doi.org/10.1080/00397911.2010.515367
Publikováno v:
Synthetic Communications. 41:1247-1250
A facile one-pot synthesis of ethyl esters from aldehydes has been developed. This tandem process involves the formation of a nitrile intermediate obtained from the reaction of an aldehyde with hydroxylamine hydrochloride in dimethylsulfoxide (DMSO)
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::87d57b772bd1546a3076e74a0f9b856f
https://doi.org/10.1080/00397911.2010.481749
https://doi.org/10.1080/00397911.2010.481749
Autor:
Robert C. Mebane, Samuel T. Chill
Publikováno v:
Synthetic Communications. 40:2014-2017
A facile one-pot synthesis of amides from aldehydes has been developed. This tandem process involves the formation of a nitrile intermediate obtained from the reaction of an aldehyde with hydroxylamine hydrochloride in dimethylsulfoxide at 100°C and
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::a6101accb97c1fde5e2bf5ab071bf235
https://doi.org/10.1080/00397910903219443
https://doi.org/10.1080/00397910903219443
Autor:
Robert C. Mebane, Kimberly L. Holte, Nathanael K. Kokes, Katherine J. Wert, Daniel R. Zuidema, Samuel T. Chill, Sarah L. Williams
Publikováno v:
Synthetic Communications. 40:1187-1191
Ketones are readily reduced to secondary alcohols with sodium hydroxide in refluxing isopropanol.
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::77169d85be56cedcf99557c8587208eb
https://doi.org/10.1080/00397910903061043
https://doi.org/10.1080/00397910903061043
Publikováno v:
Synthetic Communications. 38:3810-3815
Aldoximes are readily dehydrated to nitriles with Raney nickel in refluxing 2-propanol.
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::1553e30185862a90c47ae174d41bd8e1
https://doi.org/10.1080/00397910802238676
https://doi.org/10.1080/00397910802238676
Publikováno v:
Synthetic Communications. 37:2787-2791
Raney nickel in refluxing 2-propanol containing 2% KOH is an effective catalytic system for reducing nitriles to amines.
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::347aac132640070a28a4c9946e7ec847
https://doi.org/10.1080/00397910701481211
https://doi.org/10.1080/00397910701481211
Autor:
Robert C. Mebane, Amanda J. Mansfield
Publikováno v:
Synthetic Communications. 35:3083-3086
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::49a31627b179bdd83d55c80562546af0
https://doi.org/10.1080/00397910500281028
https://doi.org/10.1080/00397910500281028
Publikováno v:
Applied Catalysis A: General. 219:281-289
Raney nickel in refluxing 2-propanol is an effective catalytic system for cleaving C–O bonds in aromatic alcohols by transfer hydrogenolysis. Deoxygenation of alcohols substituted at the -, -, -, -, and e-positions was accomplished. The reaction ap
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::58386804e7de26c0da690023e4f77e5e
https://doi.org/10.1016/s0926-860x(01)00700-1
https://doi.org/10.1016/s0926-860x(01)00700-1
Publikováno v:
Tetrahedron Letters. 40:1459-1462
Reaction of diethyl dibromomalonate ( 1 ) with sodium methoxide in cyclohexene yields dibromonorcarane ( 2 ) as the major product. This product forms via the capture of dibromocarbene ( 4 ) by cyclohexene. Dibromocarbene, in turn, is generated from e
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::3b3af6abae9eefb0edf7ad2738e98898
https://doi.org/10.1016/s0040-4039(99)00024-6
https://doi.org/10.1016/s0040-4039(99)00024-6