Zobrazeno 1 - 7
of 7
pro vyhledávání: '"Robert A. Martuch"'
Publikováno v:
Journal of Coordination Chemistry. 56:307-312
The synthesis and structural characterization of a novel ionic Ga(III) five coordinate complex [{CH3(C5H4N)}Ga(SCH2(CO)O)2]-[(4-MepyH)]+, (4-Mepy = CH3(C5H5N)) from the reaction between Ga2Cl4 with sodium mercapto-acetic acid in 4-methylpyridine is d
Autor:
Kulbinder K. Banger, Philip E. Fanwick, Aloysius F. Hepp, Stan A. Duraj, Robert A. Martuch, David G. Hehemann
Publikováno v:
Journal of Coordination Chemistry. 55:1427-1431
The synthesis and structural characterization of a novel In(III) complex is described. The reaction between InCl3 with sodium mercapto-acetic acid, (NaSCH2(CO)OH) in 4-methylpyridine, (CH3(C5H5N), (4-Mepy)) at 25 C affords [ClIn(SCH2(CO)O)2]2- [(4-Me
Autor:
Robert A. Martuch, Michal Sabat, Aloysius F. Hepp, William E. Eckles, Robert M. Richman, Maria T. Andras, Stan A. Duraj, Hall L. Moore
Publikováno v:
Journal of Cluster Science. 7:199-210
The title compound, Cu4S10(4-methylpyridine)(sub 4) (dot) 4-methylpyridine was prepared by three different reactions: the oxidation of copper powder by sulfur and the reaction of copper (I) sulfide (or CuBr (dot) SMe2) with excess sulfur, both in the
Autor:
R. W. Binkley, Robert L. R. Towns, Ronald J. Baker, R. Huff, M. Skladany, M. J. Jedrzejas, Xiaogao Liu, Zhenhua Chen, N. Adair, M. Andras, Robert A. Martuch, F. Anwari
Publikováno v:
Acta Crystallographica Section C Crystal Structure Communications. 49:481-483
C 21 H 23 BrO 7 S, M r =499.37, monoclinic, P2 1 , a=8.897 (3), b=8.213 (2), c=15.334 (4) A, β=102.69 (3) o , V=1093 (1) A 3 , Z=2, D m =1.51, D x =1.517 g cm -3 , λ(Mo Kα)=0.71073 A, μ=19.89 cm -1 , F(000)=512, T=295 K, final R=0.044, wR=0.048 f
Publikováno v:
Acta Crystallographica Section C Crystal Structure Communications. 49:548-550
γ-Picolinium bromide, [C 6 H 7 NH]Br, M r =174.05, monoclinic, Cm, a=8.785 (4), b=8.318 (3), c=4.920 (1) A, β=103.62 (3) o , V=349.4 (4) A 3 , Z=2, D x =1.654 g cm -3 , λ(Mo Kα)=0.71073 A, μ=57.23 cm -1 , F(000)=172, T=293 K, R=0.033 for 415 ref
Autor:
Aloysius F. Hepp, M. J. Jedrzejas, Robert L. R. Towns, Stan A. Duraj, Robert A. Martuch, Ronald J. Baker
Publikováno v:
Acta Crystallographica Section C Crystal Structure Communications. 49:536-538
Bromobis(4-methylpyridine)copper(I), [CuBr(C 6 H 7 N) 2 ], M r =329.71, triclinic, P1, a=9.254 (7), b=9.736 (3), c=7.955 (3) A, α=102.34 (3), β=112.33 (3), γ=95.09 (4) o , V= 636.2 (6) A 3 , Z=2, D m =1.8, D x =1.721 g cm -3 , λ(Mo Kα)=0.710326
Autor:
Aloysius F. Hepp, Robert A. Martuch, Stan A. Duraj, M.T. Andras, E. M. Gordon, Phillip E. Fanwick
Publikováno v:
Acta Crystallographica Section C Crystal Structure Communications. 52:1701-1702
4-Methylpyridinium hydrogen sulfide, C 6 H 7 NH + .HS - , was obtained as a by-product of the reaction between GaCl 3 and thioglycolic acid in a 4-methylpyridine solution. The compound consists of heterocyclic C 6 H 7 NH + cationic rings and HS - ani