Výsledky vyhledávání - "Ralph Stähler"

Four New Thioantimonates(III) with the General Formula [TM(tren)]Sb4S7 (TM = Mn, Fe, Co, Zn) with the Transition Metal as Part of a Thioantimonate(III) Network Synthesized under Solvothermal Conditions and Tuning of the Optical Band Gap by the Transition Metal Cation

Autor: Christian Näther, Wolff‐Ragnar Kiebach, Ralph Stähler, Wolfgang Bensch, Michael Schaefer

Publikováno v: Zeitschrift f�r anorganische und allgemeine Chemie. 630:1816-1822

Four new thioantimonate(III) compounds with the general formula [TM(tren)]Sb4S7, TM = Mn 1, Fe 2, Co 3 and Zn 4, were synthesized under solvothermal conditions by reacting elemental TM, Sb and S in an aqueous solution of tren (tren = tris(2-aminoethy

Externí odkaz: https://explore.openaire.eu/search/publication?articleId=doi_________::2dd26c73c9e9e58df24496b54ae72b56
https://doi.org/10.1002/zaac.200400124

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Solvothermal syntheses, crystal structures, and thermal stability of two new thioantimonates(III) using complex transition metal cations as structure directing agents: the layered compound [Ni(dien)2]Sb4S7·H2O and the three-dimensional compound [Ni(dien)2]3Sb12S21·H2O

Autor: Wolfgang Bensch, Christian Näther, Ralph Stähler

Publikováno v: Journal of Solid State Chemistry. 174:264-275

The two new thioantimonates(III) [Ni(dien)2]Sb4S7·H2O (I) and [Ni(dien)2]3Sb12S21·H2O (II) were prepared under solvothermal conditions using elemental Ni, Sb, S and an aqueous solution of diethylenetriamine (dien) as solvent. Compound I crystallize

Externí odkaz: https://explore.openaire.eu/search/publication?articleId=doi_________::a7259f15eb3a75a5d655bbcfca146c5a
https://doi.org/10.1016/s0022-4596(03)00216-0

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Two new [Ni(tren)2]2+complexes: [Ni(tren)2]Cl2and [Ni(tren)2]WS4

Autor: Ralph Stähler, Jan Ellermeier, Wolfgang Bensch

Publikováno v: Acta Crystallographica Section C Crystal Structure Communications. 58:m70-m73

Both title compounds, bis[tris(2-aminoethyl)amine]nickel(II) dichloride, [Ni(tren)(2)]Cl(2), (I), and bis[tris(2-aminoethyl)amine]nickel(II) tetrathiotungstate, [Ni(tren)(2)]WS(4), (II), contain the [Ni(tren)(2)](2+) cation [tren is tris(2-aminoethyl

Externí odkaz: https://explore.openaire.eu/search/publication?articleId=doi_dedup___::602c33fdc6836c89b060cd548c3a37f6
https://doi.org/10.1107/s0108270101015992

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The Hydrothermal Synthesis, Crystal Structures and Thermal Stability of the Novel One- and Two-Dimensional Thioantimonate(III) Compounds [Co(tren)]Sb2S4 and [Ni(tren)]Sb2S4

Autor: Ralph Stähler, Wolfgang Bensch

Publikováno v: European Journal of Inorganic Chemistry. 2001:3073-3078

Two novel thioantimonate(III) compounds [Co(C6H18N4)]Sb2S4 (1) and [Ni(C6H18N4)]Sb2S4 (2) were synthesised under solvothermal conditions by reacting the transition metal, Sb and S in a 50% solution of tris(2-aminoethyl)amine (tren). The use of a tetr

Externí odkaz: https://explore.openaire.eu/search/publication?articleId=doi_________::8d0b2f6d85e1ed8551160babbb4a44c8
https://doi.org/10.1002/1099-0682(200112)2001:12<3073::aid-ejic3073>3.0.co

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Thioantimonate(III) anions acting as bridging ligands in neutral transition metal complexes: solvothermal synthesis and characterisation of the two novel compounds [Co(C6H18N4)]2Sb4S8 and [Co(C6H18N4)]2Sb2S5 containing [Sb4S8]4– and [Sb2S5]4– anions

Autor: Wolfgang Bensch, Ralph Stähler

Publikováno v: Journal of the Chemical Society, Dalton Transactions. :2518-2522

The two novel thioantimonate(III) compounds [Co(C6H18N4)]2Sb4S81 and [Co(C6H18N4)]2Sb2S52 were synthesised under solvothermal conditions by reacting elemental Co, Sb and S in a 95% solution of tris(2-aminoethyl)amine (tren). Compound 1 crystallises i

Externí odkaz: https://explore.openaire.eu/search/publication?articleId=doi_________::9dd8cae804e2ffe39c768eb81bc5a170
https://doi.org/10.1039/b102273n

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Tris{bis[N-(2-aminoethyl)-1,2-ethanediamine-κ3N]nickel(II)} bis(tetrathioantimonate)

Autor: Christian Näther, Ralph Stähler, Wolfgang Bensch

Publikováno v: Acta Crystallographica Section C Crystal Structure Communications. 57:26-27

Yellow crystals of [Ni(deta)2]3[SbS4]2 (deta is diethylenetriamine, C4H13N3) were synthesized under solvothermal conditions by reacting elemental Ni, Sb and S in a solution of diethylenetriamine. The structure is composed of tetrahedral [SbS4

Externí odkaz: https://explore.openaire.eu/search/publication?articleId=doi_dedup___::98463e243aa276b3b8039a91e5571b5f
https://doi.org/10.1107/s0108270100014359

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Solvothermal synthesis of [Ni(C4H13N3)2]2Sb4S8: the first compound with a cyclic [Sb4S8]4− anion

Autor: Wolfgang Bensch, Ralph Stähler, Christian Näther

Publikováno v: Chemical Communications. :477-478

Under mild hydrothermal conditions the novel thioantimonate(III) [Ni(C4H13N3)2]2Sb 4S8 was synthesised using elemental nickel, antimony and sulfur; the structure is composed of cyclic isolated [Sb4S8]4− anions and [Ni(C4H13N3)2]2+ cations.

Externí odkaz: https://explore.openaire.eu/search/publication?articleId=doi_________::98f129a6435b9f91936f633b22c549a4
https://doi.org/10.1039/b009583o

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Solvothermal Synthesis and Crystal Structure of the New Layered Thioantimonate(III) [Ni(C4H13N3)2]9Sb22S42 · 0.5H2O: Interconnection of the SbS3, SbS4, and SbS5 Primary Building Units Yielding the Very Large Sb30S30 HeteroringDedicated to Professor Welf Bronger on the Occasion of his 70th Birthday

Autor: Wolfgang Bensch, Ralph Stähler

Publikováno v: Zeitschrift für anorganische und allgemeine Chemie. 628:1657

The novel thioantimonate(III) [Ni(dien)2]9Sb22S42 · 0.5H2O was synthesised under solvothermal conditions by reacting elemental Ni, Sb and S in an aqueous solution of diethylenetriamine (dien) (80%). The compound crystallises in the triclinic space g

Externí odkaz: https://explore.openaire.eu/search/publication?articleId=doi_________::33910ea2246a6f83efb996d7deeb037d
https://doi.org/10.1002/1521-3749(200207)628:7<1657::aid-zaac1657>3.0.co

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