Zobrazeno 1 - 10
of 517
pro vyhledávání: '"ROBIN K. HARRIS"'
The power of nuclear magnetic resonance, NMR, for characterizing molecules dissolved in solution is widely acknowledged and NMR forms an essential component of undergraduate chemistry degrees. However, the application of NMR to the solid state is muc
Autor:
Robin K. Harris, Stephen Byard, Andrew J. Ilott, Vadim Zorin, Anuji Abraham, David C. Apperley, Paul Hodgkinson, Andrew J. Robbins
Publikováno v:
CrystEngComm, 2016, Vol.18(6), pp.1054-1063 [Peer Reviewed Journal]
A combination of solid-state NMR techniques, including 13C/1H correlation, 2H magic-angle spinning NMR and first principles calculation are employed to characterise the role of water in different hydration states of sildenafil citrate. The 13C spectr
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_dedup___::48f4cea8335bdea95ec13023e303bfcb
https://doi.org/10.1039/c5ce02234g
https://doi.org/10.1039/c5ce02234g
Autor:
Ram K. R. Jetti, Volker Kahlenberg, David C. Apperley, Thomas Gelbrich, Robin K. Harris, Neslihan Zencirci, Ulrich J. Griesser
Publikováno v:
The Journal of Physical Chemistry B. 118:3267-3280
The solvent formation of phenobarbital, an important drug compound with an unusually complex polymorphic behavior, was studied in detail. Monosolvates with acetonitrile, nitromethane, dichloromethane, and 1,4-dioxane were produced and characterized b
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_dedup___::bb0a5d503860fac852a95e9fe83c26db
https://doi.org/10.1021/jp409201v
https://doi.org/10.1021/jp409201v
NMR in Pharmaceutical Sciences is intended to be a comprehensive source of information for the many individuals that utilize MR in studies of relevance to the pharmaceutical sector. The book is intended to educate and inform those who develop and ap
Publikováno v:
Magnetic Resonance in Chemistry. 50:680-690
The solid-state structures of two polymorphs and two alcoholates (ethanol and isopropanol) of formoterol fumarate have been investigated by a combination of NMR techniques. First-principles shielding computations are combined with NMR data to success
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::21d07260ec69f3b474e8f5b5d5e04105
https://doi.org/10.1002/mrc.3862
https://doi.org/10.1002/mrc.3862
Autor:
Stewart J. Clark, Paul Hodgkinson, Andrei S. Batsanov, Robin K. Harris, Dominik B. Jochym, David C. Apperley
Publikováno v:
Journal of Molecular Structure. 1015:192-201
The validity of the structure of diterbutaline sulphate diacetic acid solvate in the Cambridge Crystallographic Database (code ZIYXAG) was checked using 13C solid-state NMR together with shielding computations and was found to be in error as far as t
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::525dee5308e7d026094f6bb5fbbc19d9
https://doi.org/10.1016/j.molstruc.2011.10.024
https://doi.org/10.1016/j.molstruc.2011.10.024
Publikováno v:
Journal of Pharmaceutical Sciences. 101:176-186
The dehydration/desolvation of two hydrate solvates of the pharmaceutically important compound finasteride (namely, bisfinasteride monohydrate monotetrahydrofuran and bisfinasteride monohydrate mono-1,4-dioxane) has been studied by solid-state nuclea
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_dedup___::c246d31c0e388113b714ca1cc167db02
https://doi.org/10.1002/jps.22740
https://doi.org/10.1002/jps.22740
Autor:
Volker Kahlenberg, Thomas Gelbrich, Ulrich J. Griesser, Robin K. Harris, Neslihan Zencirci, David C. Apperley
Publikováno v:
Crystal Growth & Design. 10:302-313
Six of the more easily accessible forms of phenobarbital (Pbtl-I, II, III, IV, V, VI) were characterized by a variety of analytical methods (thermal analysis, solution calorimetry, X-ray diffraction methods, infrared, Raman and solid-state NMR spectr
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::8d82af556ee58c11ded674d2715096af
https://doi.org/10.1021/cg901062n
https://doi.org/10.1021/cg901062n
Autor:
Alan Wong, Jonathan R. Yates, Robin K. Harris, Mark E. Smith, Lindsay S. Cahill, John V. Hanna, Jair C. C. Freitas
Publikováno v:
Chemistry - A European Journal. 15:9785-9798
Solid-state (25)Mg magic angle spinning nuclear magnetic resonance (MAS NMR) data are reported from a range of organic and inorganic magnesium-oxyanion compounds at natural abundance. To constrain the determination of the NMR interaction parameters (
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_dedup___::fe364b500c15cc213a7be03cfd286e8e
https://doi.org/10.1002/chem.200900346
https://doi.org/10.1002/chem.200900346
Use of rotary echoes in 2H magic-angle spinning NMR for the quantitative study of molecular dynamics
Publikováno v:
Chemical Physics Letters. 475:58-63
The interaction of sample spinning and chemical dynamics is analysed in the context of 2 H magic-angle spinning NMR. We develop previous analyses and show that a metric based on the intensity of rotational echoes allows kinetic information to be deri
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::e7154b90fb14f63d9a7f3a212e6bc0ce
https://doi.org/10.1016/j.cplett.2009.05.031
https://doi.org/10.1016/j.cplett.2009.05.031