Zobrazeno 1 - 10
of 24
pro vyhledávání: '"R. Rao Gadde"'
Autor:
R. Rao Gadde, James E. DiNunzio
Publikováno v:
Journal of Chromatography A. 594:209-216
This paper reports on the development of high-performance liquid chromatographic methods for the determination of hydroxamic acids in topical formulations. A poly(styrene-divinylbenzene)copolymer stationary phase with a mobile phase of acetonitrile a
Autor:
R. Rao Gadde, Frederick W. Burton
Publikováno v:
Journal of Chromatography A. 593:41-46
An isocratic reversed-phase high-performance liquid chromatographic method for the analysis of 13-cis-retinoic acid in serum is developed. Sample preparation includes deproteination with acetonitrile-perchloric acid-acetic acid followed by centrifuga
Publikováno v:
Journal of Pharmaceutical and Biomedical Analysis. 9:1031-1036
Chlorhexidine phosphanilate (CHP) is analysed by two separate reversed-phase HPLC methods. CHP was found to be a non-stoichiometric compound with a phosphanilic acid to chlorhexidine ratio of 1.83. By careful choice of solvents, solution pH and HPLC
Publikováno v:
Journal of Chromatography A. 522:227-234
A stability indicating reversed-phase high-performance liquid chromatographic method has been developed to quantify tretinoin (all- trans -retinoic acid) in cream formulations. Tretinoin cream samples were dissolved directly in tetrahydrofuran and di
Autor:
R. Rao Gadde, Frederick W. Burton
Publikováno v:
Journal of Chromatographic Science. 28:543-546
A method is described to determine the purity of 13-cis-retinoic acid. Spectrophotometry is used to determine the non-UV-absorbing impurities, and HPLC is used to determine the UV-absorbing impurities. In combination, these methods permit determinati
Autor:
R. Rao Gadde, James E. DiNunzio
Publikováno v:
Journal of Chromatography A. 519:117-124
A method for the determination of sunscreen compounds in over-the-counter topical sunscreen products is described. The method uses reversed-phase liquid chromatography with an eluent of tetrahydrofuran and dilute acetic acid. The analytes are detecte
Autor:
Federick W. Burton, R. Rao Gadde
Publikováno v:
Journal of Chromatography A. 328:317-324
A reversed-phased liquid chromatographic methods is described for the determination of anthralin in topical products. The factors affecting the degradation of anthralin solid and solutions are discussed. Ultraviolet spectra of degradation products ar
Autor:
Haiyung Cheng, R. Rao Gadde
Publikováno v:
Journal of Chromatographic Science. 23:227-230
Discussion de quelques artefacts dans un detecteur HP 1040A, et proposition de quelques modifications de routines
Autor:
R. Rao Gadde, Haiyung Cheng
Publikováno v:
Journal of Chromatography A. 355:399-406
A stability-indicating high-performance liquid chromatographic method using an amine column and a UV detector at 214 nm is developed for lactic acid in dermatological products. The detector response for lactic acid is linear in the range 8.8–39.9
Autor:
R. Rao Gadde, Herbert A. Laitinen
Publikováno v:
Analytical Chemistry. 46:2022-2026