Zobrazeno 1 - 8
of 8
pro vyhledávání: '"Philip J. Oles"'
Autor:
Philip J Oles
Publikováno v:
Journal of AOAC INTERNATIONAL. 76:615-620
Experimental designs based on procedures of Taguchi are described for optimizing analytical methods. Methods were efficiently developed, with improvements in precision and accuracy, for the determination of cholesterol in foods, magnesium in feed pre
Autor:
Seth Kensinger, Gloria Gates, Philip J Oles, David Schumacher, Arlene Silcox, Tammy Showers, Jacqueline Patchell
Publikováno v:
Journal of AOAC INTERNATIONAL. 73:724-728
A fractional factorial (Taguchi) experiment was designed to optimize recovery of cholesterol from a baked food matrix. A pretzel sample was chosen for the spiking design experiment. Factors studied Include the alcohol used for saponification, the ext
Autor:
Wanda M Graham, Philip J Oles
Publikováno v:
Journal of AOAC INTERNATIONAL. 74:812-814
Food matrixes were digested by treatment with nitric acidsulfuric acid-hydrogen peroxide mixtures and heating with a commercially available microwave apparatus. The digests were analyzed for sodium, potassium, magnesium, iron, calcium, zinc, copper,
Autor:
Philip J. Oles
Publikováno v:
Journal of Chemical Education. 75:357
Fractional factorial experimental design is introduced as a group laboratory exercise in quantitative analysis. The classical gravimetric determination of chloride by precipitation with silver ion serves as the basis for this work. Using the designs
Autor:
Philip J. Oles, Sidney. Siggia
Publikováno v:
Analytical Chemistry. 46:2197-2200
Autor:
Philip J. Oles, Sidney. Siggia
Publikováno v:
Analytical Chemistry. 46:911-914
Autor:
Philip J. Oles
Publikováno v:
Journal of Pharmaceutical Sciences. 67:1300-1302
A high-pressure liquid chromatographic assay for streptozocin in a sterile powder formulation (1.0 g/vial) is described. The method effectively separates the alpha- and beta-anomeric forms of streptozocin. Quantitative results are presented for the d
Autor:
Philip J. Oles, Sidney. Siggia
Publikováno v:
Analytical Chemistry. 45:2150-2151