Zobrazeno 1 - 10
of 11
pro vyhledávání: '"Patrizia Leogrande"'
Autor:
Patrizia Leogrande, Daniel Jartdines, Dayamin Martinez‐Brito, Xavier de la Torre, Maria Kristina Parr, Francesco Botrè
Publikováno v:
Rapid Communications in Mass Spectrometry. 37
Autor:
Xavier De la Torre, Dayamin Martinez Brito, Francesco Donati, Francesco Botre, Patrizia Leogrande
Publikováno v:
Drug Testing and Analysis. 14:1438-1450
This paper aimed to assess a method to measure eight thyroid-related compounds in serum by liquid chromatography-mass spectrometry (LC-MS/MS), to verify the correlation with radioimmunoassay (RIA), to evaluate the possible cross-reactivity, and to ob
Publikováno v:
SSRN Electronic Journal.
Thyroid hormones and their derivatives are structurally related to the non-essential amino acid tyrosine (4-hydroxyphenylalanine). However, there are physicochemical differences that make it difficult to apply an analytical method for their simultane
Autor:
Patrizia Leogrande, Daniel Jardines, Maria Kristina Parr, X. de la Torre, Francesco Botrè, Dayamin Martinez-Brito, E. Domenici
Publikováno v:
Rapid Communications in Mass Spectrometry. 36
RATIONALE This work demonstrated the high potential of combining high-resolution mass spectrometry with chemometric tools, using metabolomics as a guided tool for anti-doping analysis. The administration of 7-keto-DHEA was studied as a proof-of-conce
Autor:
Maria Kristina Parr, Francesco Botrè, Dayamin Martinez-Brito, Daniel Jardines, Patrizia Leogrande, Xavier de la Torre
Publikováno v:
Rapid Communications in Mass Spectrometry. 35
RATIONALE Systematic electron ionization fragmentation studies of steroids have been performed to elucidate and trace their characteristic fragmentation patterns. However, the electron ionization source setting at 70 eV electron energy is much higher
Autor:
Francesco Botrè, Davide Curcio, Patrizia Leogrande, Xavier de la Torre, Cristiana Colamonici, Dayamin Martinez Brito
Publikováno v:
Drug testing and analysisREFERENCES. 13(7)
RATIONALE The instability of androst-5-ene-3,7-dione structures under acidic conditions is known. The formation of arimistane from 7-oxo-DHEA, influenced by the conditions of sample extraction, and mainly derivatization reaction and gas chromatograph
Publikováno v:
Rapid communications in mass spectrometry : RCMREFERENCES. 35(12)
Rationale The metabolism of arimistane (Arim) was first described in 2015, and androst-3,5-diene-7β-ol-17-one was proposed as the main metabolite excreted in urine. Recently, a more detailed study describing the findings in urine after the administr