Zobrazeno 1 - 10
of 20
pro vyhledávání: '"Octave J Francis"'
Autor:
Glenn A. Bennett, Allen S Carman, George M Ware, Octave J Francis, Shia S. Kuan Pesi Umrigar, Lawrence Carter
Publikováno v:
Analytical Letters. 26:1751-1770
A method is described for the determination of fumonisin B1 in corn. The method involves sample extraction with methanol:water (75:25) and partial purification using a solid phase extraction. Fumonisin B1 is reacted with naphthalene-2,3-dicarboxaldeh
Publikováno v:
Journal of Agricultural and Food Chemistry. 38:185-190
La methode permet un dosage des phytoestrogenes par chromatographie HPLC dans le soja et produits derives, sans delipidation selon le type de detection, UV ou fluorescence, la limite de detection est de 0.5 a 2 p.p.m.
Publikováno v:
Journal of Agricultural and Food Chemistry. 34:279-282
Publikováno v:
Journal of AOAC INTERNATIONAL. 67:1095-1098
A sensitive, highly selective liquid chromatographic (LC) method is described which uses electrochemical (EC) reduction of the analyte in the determinative step. The method is capable of determining xanthomegnin in mixed animal feeds and grains at le
Publikováno v:
Analytical Letters. 22:2335-2352
A method is described for the determination of zearalenol and zearalenone in corn using electrochemical detection. the sample is extracted with chloroform, and the extract is cleaned up by liquid-liquid partition. Zearalenol and zearalenone are resol
Autor:
Octave J Francis
Publikováno v:
Journal of AOAC INTERNATIONAL. 62:1182-1185
A procedure has been devised for more rapid preparation of large samples of nutmeats (10-80 lb) for mycotoxin analysis without the use of grinding aids, by combining the grinding and mixing steps into one operation. Ease of cleaning equipment facilit
Publikováno v:
Journal of AOAC INTERNATIONAL. 67:731-734
A method is described for the determination of deoxynivalenol (DON) in wheat. The method involves sample extraction with chloroformethanol (8 + 2), column chromatographic cleanup on silica gel of small particle size, and derivatization with heptafluo
Publikováno v:
Journal of AOAC INTERNATIONAL. 59:118-121
A total of 315 marketable and 57 obviously damaged corn samples were collected at 116 different farms and country elevators located in the United States in counties selected from among those producing more than 1 million bushels of corn in 1972. The
Publikováno v:
Analytical Letters. 18:837-846
A derivatization procedure was developed for the fluorometric determination of purified xanthomegnin. A highly fluorescent product is formed by reaction of xanthomegnin with ammonia and hydrogen peroxide under defined conditions. The derivative is a
Publikováno v:
Journal of AOAC INTERNATIONAL. 66:587-591
A high pressure liquid chromatographic (HPLC) method is described for the determination of xanthomegnin in grains and mixed animal feeds at levels ranging from 150 to 1200 ng/g. This is equivalent to actual amounts of xanthomegnin injected on the HPL