Zobrazeno 1 - 10
of 33
pro vyhledávání: '"O. Ya. Borbulevych"'
Autor:
A. N. Shchukin, O. Ya. Borbulevych, O. I. Boikova, G. V. Grintselev-Knyazev, I. E. Yakunina, O. V. Leonova, I. V. Shakhkel'dyan, Yu. M. Atroshchenko, E. N. Alifanova, V. A. Subbotin
Publikováno v:
Russian Journal of Organic Chemistry. 39:1593-1602
By condensation of 2,4-bis(aci-nitro)-3-(2-phenyl-2-oxoethyl)cyclohex-5-en-1-one with formaldehyde and primary amines a series of N-substituted 9-(2-phenyl-2-oxoethyl)-1,5-dinitro-3-azabicyclo[3.3.1]non-7-en-6-ones was synthesized. With the use of X-
Publikováno v:
Russian Chemical Bulletin. 50:1064-1067
Condensation of ortho-aminophenols and N-benzylsulfonyl-o-phenylenediamine with ninhydrin afforded tetracyclic products, the amino group entering into condensation with the carbonyl group at position 1 of ninhydrin. The structures of the reaction pro
Autor:
O. Ya. Borbulevych, Oleg V. Shishkin, V. M. Mamaev, N. G. Akhmedov, S. S. Gitis, P. V. Chudakov, E. N. Alifanova, M. Yu. Antipin, Igor P. Gloriozov, Yu. M. Atroshchenko, A. Ya. Kaminsky, Yu. D. Grudtsyn
Publikováno v:
Russian Chemical Bulletin. 50:1056-1063
The reactions of the acetonate ion with 1,3-dinitro-5-X-, 1,3-X2-5-nitro- (X = NO2, CN, COOCH3, CONH2, COO–, and H), and 1,3,5-tricyanobenzenes were studied by 1H NMR and electronic absorption spectroscopy and by quantum-chemical methods. The kinet
Autor:
O. Ya. Borbulevych, M. Yu. Antipin, A. E. Ruzhnikov, Sergey V. Kurbatov, L. P. Olekhnovich, A. V. Lesin
Publikováno v:
Russian Chemical Bulletin. 50:1264-1267
A new preparative procedure was developed for the synthesis of spiro-fused 1,4-benzothiazines by thermal heterocyclization of S-benzyl and S-phenacyl derivatives of o-indothiophenol.
Publikováno v:
Russian Chemical Bulletin. 49:732-735
The reactions of 4-morpholino-1,2-naphthoquinone with enamines, cyclohexanone derivatives, afford 7a-amino-5-morpholinohexahydrobenzo[b]naphtho[1,2][1,4]dioxines, while the reaction witho-phenylenediamine yields 5-morpholinobenzo[a]phenazine.
Publikováno v:
Journal of Molecular Structure. 520:141-153
Molecular structure and conformational flexibility of Meisenheimer complexes of 5,7-dinitroquinoline derivatives are studied experimentally using X-ray diffraction and theoretically by semi-empirical AM1 calculations. The dihydrocycle is found to pos
Publikováno v:
Russian Chemical Bulletin. 49:452-459
The electron density distribution in the crystal of the Meisenheimer complex of potassium 3-methyl-5′, 7′-dinitro-5′, 8′-dihydrospiro(1,3-oxazolidine-2,8′- quinolinide) (1) was studied based on the data of precision X-ray diffraction study.
Publikováno v:
Acta Crystallographica Section C Crystal Structure Communications. 55:1915-1918
In molecules of the title compound, C 14 H 10 N 4 O 6 S, the geometry of the six-membered ring is typical for Meisenheimer complexes of 2,4,6-trinitrobenzene. However, the difference between the C-N bond lengths of the nitro groups para and ortho to
Autor:
Oleg V. Shishkin, Alexander N. Shchegolikhin, O. Ya. Borbulevych, Yu. G. Gololobov, I. R. Golding, W. Gruber, Pavel V. Petrovskii
Publikováno v:
Russian Chemical Bulletin. 48:924-928
N-Substituted amides of 2-cyanopenta-2E,4-dienoic acid were synthesized by condensation ofN-substituted cyanoacetamides with acrolein in a dioxane-DMSO solution in the presence of Zn(OAc)2·2H2O as a condensing agent. X-ray diffraction study of 3-met
Publikováno v:
Russian Chemical Bulletin. 48:561-566
Benzimidazole-2-carbaldehyde reacts with 1-morpholinocyclohexene, 1-morpholinocyclopentene, and aminocrotonic ester upon heating to form 4a,11-dimorpholino-1,2,3,4,11,11a-hexahydro-4aH-indolo[1,2-a]benzimidazole, 2-(2-morpholino-4,5-dihydrofulvenyl)b