Zobrazeno 1 - 10
of 25
pro vyhledávání: '"O. B. Lapina"'
Publikováno v:
Physical chemistry chemical physics : PCCP. 22(28)
A sample with a nominal composition 'NaVPO4F' is prepared by mechanochemically assisted solid-state synthesis using quenching. A detailed study of its crystal and local structure is conducted by means of XRD and FTIR and solid-state 31P NMR spectrosc
Autor:
V. P. Isupov, M. R. Sharafutdinov, D. F. Khabibulin, L. E. Chupakhina, O. B. Lapina, O. A. Kharlamova
Publikováno v:
Inorganic Materials. 47:763-767
The structural transformations accompanying the mechanochemical synthesis of fine-particle γ-LiAlO2 have been studied by 6Li and 27Al NMR and in situ X-ray diffraction. Mechanical activation of a mixture of aluminum hydroxide and lithium carbonate i
Autor:
L. N. Gal, Yu. V. Smetannikov, A. N. Lupanov, Natalia Tarasova, D. F. Khabibulin, O. B. Lapina
Publikováno v:
Theoretical Foundations of Chemical Engineering. 42:657-661
Phosphorus- and sulfur-containing polymers were obtained by radiation-chemical synthesis from elementary phosphorus and sulfur in benzene. The structure and composition of the products were studied by solid-phase 31P NMR spectroscopy, MALDI mass spec
Publikováno v:
Progress in Nuclear Magnetic Resonance Spectroscopy. 53:128-191
Autor:
A. Ya. Rozovskii, Rimma Bunina, E.A. Paukshtis, Alexander M. Volodin, Vladislav A. Sadykov, V. V. Lunin, I. V. Yudaev, V. F. Tret’yakov, N. V. Mezentseva, D. A. Ziuzin, O. B. Lapina, Galina Alikina, V. P. Doronin, Ella M. Moroz, V. B. Fenelonov, V. N. Kolomiichuk, Tatiana Kuznetsova, Julian R.H. Ross, Tatyana N. Burdeynaya, D. I. Kochubei, B. N. Novgorodov, Valery A. Matyshak
Publikováno v:
Topics in Catalysis. 32:29-38
Approaches to design of zirconia pillared clays via control of the properties of pillaring species in solutions were elaborated. Structural features of pillars and Pt + Cu active components fixed at these nanoparticles were shown to determine catalyt
Publikováno v:
Glass Physics and Chemistry. 28:1-4
The structure of sulfate–phosphate glasses is investigated by high-resolution 31P solid-state nuclear magnetic resonance with magic-angle sample spinning (31P MAS NMR spectroscopy). The structure parameters that account for the number of different
Autor:
H. J. Eberle, Peter Behrens, Bernd Pillep, Helmut Knözinger, J. Spengler, Eric Bosch, O. B. Lapina, F. Anderle, R. K. Grasselli, A. A. Shubin
Publikováno v:
The Journal of Physical Chemistry B. 105:10772-10783
Antimony-modified vanadia-on-titania catalysts were prepared for the selective oxidation of o-xylene to phthalic anhydride by ball milling of powder mixtures followed by calcination. A binary Sb2O3...
Autor:
Vladimir V. Zyryanov, O. B. Lapina
Publikováno v:
Inorganic Materials. 37:264-270
The products of mechanochemical synthesis in the Pb–V–O system were characterized by x-ray diffraction and magnetic resonance spectroscopy techniques. The mechanical processing was found to yield only new crystalline compounds, Pb2.67V1.33O5.96an
Publikováno v:
The Journal of Physical Chemistry B. 103:3138-3144
Milling of V2O5 in a ball mill increased the surface area from 7 to a maximum of 32 m2/g. Simultaneously, XRD line broadening suggested a reduction of the microcrystallites. A color change during milling indicated oxygen loss, and Raman spectroscopy
Publikováno v:
Chemical Physics Letters. 302:341-346
51 V static and MAS NMR spectroscopy of central transition is shown to be an effective method for the characterisation of strongly bonded V(V) species in VO x /TiO 2 catalysts. Simultaneous determination of quadrupole and CSA tensors parameters (i.e.