Zobrazeno 1 - 10
of 51
pro vyhledávání: '"N.M. Djordjevic"'
Publikováno v:
Journal of Chromatography A. 857:1-20
The separation of samples that contain more than 15 to 20 analytes (n > 15-20) is typically difficult and usually requires gradient elution. We have examined the reversed-phase liquid chromatographic separation of 24 samples with 8 < or = n < or = 48
Autor:
F. Houdiere, N.M. Djordjevic
Publikováno v:
Reviews in Analytical Chemistry, Vol 17, Iss 4, Pp 207-222 (1998)
Autor:
D.W. Hill, Lloyd R. Snyder, N.M. Djordjevic, D.L Saunders, T.J Waeghe, John W. Dolan, L. Van Heukelem
Publikováno v:
Journal of Chromatography A. 803:1-31
The optimized reversed-phase HPLC separation of 14 different samples is reported, based on simultaneous changes in temperature and gradient steepness. Four experimental runs are required for each sample, following which preferred conditions can be pr
Autor:
T.J. Waeghe, Lloyd R. Snyder, N.M. Djordjevic, Lane C. Sander, John W. Dolan, P.L. Zhu, D.W. Hill
Publikováno v:
Journal of Chromatography A. 756:21-39
It has been shown previously that computer simulation based on two initial experiments can predict separation in reversed-phase gradient elution as a function of gradient conditions (gradient steepness, gradient range and gradient shape) and column c
Autor:
L. Van Heukelem, Lane C. Sander, John W. Dolan, Jiann-Tsyh Lin, P.L. Zhu, D.W. Hill, Lloyd R. Snyder, N.M. Djordjevic
Publikováno v:
Journal of Chromatography A. 756:63-72
The separation of nine un-ionized samples was studied as a function of temperature (T) and gradient steepness (b). Selectivity values Δlog α∗ were obtained for 160 compounds, ranging from nonpolar hydrocarbons to very polar drugs. Selectivity var
Reversed- and normal-phase separations by high-temperature open-tubular column liquid chromatography
Publikováno v:
Journal of Chromatography A. 598:153-158
The selectivity and stability of some commercial reversed-phase open-tubular columns were studied under high-temperature conditions. Differently substituted chlorobenzenes were used as test compounds. Graphs of ln k′ versus the number of chlorine a
Publikováno v:
International Journal of Pharmaceutics. 81:21-29
A gas-chromatographic technique was used to measure the adsorption of water at zero and finite surface coverage of the orthorhombic form of cyclosporin A. For calculation of the surface area, the BET adsorption isotherms of water at 373 K and nitroge
Publikováno v:
Journal of Chromatography A. 592:239-247
In open-tubular liquid chromatography (OTLC), elevation of the column temperature has the same effect as reductilon of the column diameter in obtaining high column efficiencies, with the additional benefits of easier column handling and fewer problem
Autor:
N.M. Djordjevic
Publikováno v:
Thermochimica Acta. 177:109-118
Solubilities of five polycyclic aromatic hydrocarbon solids: naphthalene, acenaphthene, anthracene, phenanthrene and pyrene in n -octadecane (OD) have been determined over a range of temperatures. Differential scanning calorimetry (DSC) has been used
Publikováno v:
Journal of Chromatography A. 550:27-37
A good optimization routine should correctly find the best chromatographic separation conditions for mixtures of known or unknown constituents. The chromatographer must define the number of the parameters to be optimized and their ranges. However, th