Výsledky vyhledávání - "N. P. Volynskii"

Autor: S. E. Shevchenko, N. P. Volynskii

Publikováno v: Petroleum Chemistry. 48:123-128

A preparative procedure for the synthesis of thietanes bearing alkyl substituents in the β-position was developed. Using this procedure, 3-substituted thietanes can be obtained in four steps with an ultimate yield of > 50%. 3-R-thietanes (where R =

Externí odkaz: https://explore.openaire.eu/search/publication?articleId=doi_________::12ced7f3f0475edbd3a7e6cde3cf0bf5
https://doi.org/10.1134/s0965544108020084

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Synthesis of 2-alkyl(aryl)thietanes

Autor: S. E. Shevchenko, N. P. Volynskii

Publikováno v: Petroleum Chemistry. 47:109-117

Thietane and its 2-substituted derivatives were synthesized. A general preparation procedure for the synthesis of thietanes bearing alkyl and aryl substituents in the α-position was developed. Using this procedure, 2-substituted thietanes can be obt

Externí odkaz: https://explore.openaire.eu/search/publication?articleId=doi_________::4531242c50f152c641a60609055881cc
https://doi.org/10.1134/s0965544107020089

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ChemInform Abstract: Synthesis of 1-Substituted trans-2-Thiahydrindans and 3-Substituted trans-2-Thiadecalins

Autor: N. P. Volynskii, O. L. Alikhanova

Publikováno v: ChemInform. 23

Externí odkaz: https://explore.openaire.eu/search/publication?articleId=doi_________::645cb02d42f9349b184e13c78f8897d4
https://doi.org/10.1002/chin.199225066

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ChemInform Abstract: Synthesis of 3-Substituted trans-2-Oxadecalins (II), (IV), (V) and 1- Substituted trans-2-Oxahydrindans (VII) - (X)

Autor: O. L. Alikhanova, N. P. Volynskii

Publikováno v: ChemInform. 23

Externí odkaz: https://explore.openaire.eu/search/publication?articleId=doi_________::2b639b83d39975e2f24cf61aab6fd4c1
https://doi.org/10.1002/chin.199225067

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13C and1H NMR study of 3-R-substitutedtrans-2-oxadecalins and 1-R-substitutedcis- andtrans-2-oxahydrindans

Autor: M. B. Smirnov, N. P. Volynskii

Publikováno v: Bulletin of the Russian Academy of Sciences Division of Chemical Science. 41:668-671

Previously synthesized 3-substitutedcis- andtrans-2-oxadecalins and 1-substitutedcis- andtrans-2-oxahydrindans were studied by13C and1H NMR. The structure and configuration of these compounds were established.

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https://doi.org/10.1007/bf01150889

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Study of 1-R-substituted trans-2-thiahydrindanes and 3-R-substituted trans-2-thiadecalins by1H and13C NMR

Autor: N. P. Volynskii, M. B. Smirnov

Publikováno v: Bulletin of the Academy of Sciences of the USSR Division of Chemical Science. 40:1808-1811

1-Substituted trans-2-thiahydrindanes and 3-substituted trans-2-thiadecalins were studied by1H and13C NMR. The configurations and conformations of these compounds were established.

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https://doi.org/10.1007/bf00960408

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Synthesis of 1-substituted trans-2-thiahydrindanes and 3-substituted trans-2-thiadecalins

Autor: O. L. Alikhanova, N. P. Volynskii

Publikováno v: Bulletin of the Academy of Sciences of the USSR Division of Chemical Science. 40:1664-1671

Methods of synthesis of 1-R-trans-2-thiahydrindanes and 3-R-trans-2-thiadecalins from trans-1-methoxymethyl-2-chlorocyclohexane have been developed. The order of the chromatographic elution of the isomeric sulfides formed has been found. The configur

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https://doi.org/10.1007/bf01172271

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Synthesis of 3-substituted trans-2-oxadecalins and 1-substituted trans-2-oxahydrindanes

Autor: O. L. Alikhanova, N. P. Volynskii

Publikováno v: Bulletin of the Academy of Sciences of the USSR Division of Chemical Science. 40:1652-1663

A study was carried out of the intramolecular cyclization of trans-1-methoxymethyl-2-(1-hydroxyalkyl)cyclohexanes and trans-1-methoxymethyl-2-(2-hydroxyalkyl)cyclohexanes by the action of acid chlorides of phosphorous, sulfurous and p-toluenesulfonic

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https://doi.org/10.1007/bf01172270

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Dehydration of ethyl alcohol

Autor: N. P. Volynskii, A. I. Nekhaev, S. E. Shevchenko

Publikováno v: Russian Journal of General Chemistry. 79:326-327

Ethyl alcohol is a widely used relatively nontoxic solvent. It forms an azeotrope with water, which contains 95.5% of the alcohol. Some chemical transformations require anhydrous ethanol as reagent or solvent. A number of large-scale procedures have

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https://doi.org/10.1134/s1070363209020273

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Synthesis of 4-substituted thiacyclohexanes

Autor: N. P. Volynskii, L. P. Shcherbakova

Publikováno v: Bulletin of the Academy of Sciences of the USSR Division of Chemical Science. 28:1006-1009

1. A four-stage reaction has been developed for the synthesis of 4-alkyl(cycloalkyl, phenyl)thiacyclohexanes, starting from α-olefins. 2. The new compounds 4-hexyl-, 4-phenyl- and 4-cyclohexylthiacyclohexane and the corresponding sulfones have been

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https://doi.org/10.1007/bf00963317

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