Zobrazeno 1 - 10
of 36
pro vyhledávání: '"Mohamed Rifaat Hamza Elmoghayar"'
Publikováno v:
Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry. 17:1-13
1-Cyanoacety1-4-cinnamoylthiosemicarbazide and its complexes of the bivalent metal ions Cu(II), Ni(II), Co(II), Pb(II) and Hg(II) have been synthesised and characterized. Probable structures for the complex compounds have been proposed on the basis o
Publikováno v:
Synthesis. 1984:1-26
Revue des methodes de preparation, des etudes structurales et de la reactivite des oxo-3 alcanenitriles. Ces composes sont des intermediaires importants pour la synthese d'une variete de systemes heterocycliques difficilement accessibles par d'autres
Autor:
Mohamed Ahmed Ibrahim, Mohamed Hilmy Elnagdi, Mohamed Rifaat Hamza Elmoghayar, Mohamed Mohamed Mohamed Sallam
Publikováno v:
Helvetica Chimica Acta. 60:2171-2176
The Carbo(3-phenylpyrazol-5-yl-hydrazonoyl) halides 1a,b react with active methylene compounds to yield the 1-(3-phenylpyrazol-5-yl)-pyrazole derivatives 2a–k (Scheme 1). The acyclic intermediates 3a,b could be isolated from reaction of 1a,b with a
Publikováno v:
Monatshefte f�r Chemie Chemical Monthly. 115:1413-1419
3-Antipyrinyl-5-aminopyrazole (1) reacted with acrylonitrile to afford 5-amino-1-β-cyanoethyl-3-antipyrinylpyrazole (2). Compound2 could also be obtained from the reaction of β-cyanoethylhydrazine (3) and compound4.2 was readily cyclized into 2-ant
Autor:
Mohamed Hilmy Elnagdi, Mohamed Kamal Ahmed Ibraheim, Hikmat Hussein Alnima, Shereif Mahmoud Fahmy, Mohamed Rifaat Hamza Elmoghayar
Publikováno v:
Zeitschrift für Naturforschung B. 33:216-219
3-Phenylpyrazole-5-diazonium chloride (2) couples with benzoylacetonitrile and with phenacylthiocyanate to yield the corresponding hydrazone derivatives 3 a, b. Whereas 3 a cyclised into the pyrazolo[1,5-c]-as-triazine derivative (4a) upon treatment
Publikováno v:
Tetrahedron. 31:63-67
β-Cyanoethylhydrazine 1 reacts with benzoylacetonitrile 2 in refluxing ethanol to yield 5-amino-1-β-cyanoethyl-3-phenylpyrazole 4 ; in acetic acid acetyl-β-cyanoethylhydrazone 8 was obtained. Compounds 4 and 8 were readily cyclized into 2-phenyl-4
Publikováno v:
Monatshefte f�r Chemie Chemical Monthly. 117:201-204
The reactivity of β-cyanoethylhydrazine toward enaminonitrile and aroyl isothiocyanates is reported. A variety of 3,5-diaminopyrazole and Δ3-1,2,4-triazolin-5-thione derivatives could be prepared.
Publikováno v:
Zeitschrift für Naturforschung B. 32:307-310
The behaviour of 3,5-diamino-4-phenylazopyrazole (1) toward isothiocyanates, acrylonitrile and ethyl ethoxymethylenecyanoacetate is investigated. An improved synthesis of 4-unsubstituted-3,5-diaminopyrazoles by an arylazo removal reaction is also rep
Publikováno v:
Journal f�r Praktische Chemie. 330:657-660
Publikováno v:
Archiv der Pharmazie. 316:76-82
4-Acetylantipyrine (1) was condensed with aromatic or heterocyclic aldehydes to yield the cinnamoylidene derivatives 4a—d. Compound 4b was converted into the pyrazolinylantipyrine derivative 9 by hydrazine hydrate. 4-(Chloroacetyl)antipyrine (2) re