Zobrazeno 1 - 10
of 35
pro vyhledávání: '"Michele Ruccia"'
Autor:
Michele Ruccia, Domenico Spinelli, N. Vivona, Vincenzo Frenna, Giuseppe Cusmano, Anlonino Corrao
Publikováno v:
Journal of Heterocyclic Chemistry. 13:357-360
The rates of the mononuclear heterocyclic rearrangement of the phenylhydrazone of 3-benzoyl-5-phenyl-1,2,4-oxadiazole (1) into 2,5-diphenyl-4-benzoylamino-1,2,3-triazole (II) have heen measured in dioxane/water (50:50, v:v) in the range of pS+ 3.8–
Publikováno v:
Journal of Heterocyclic Chemistry. 12:985-988
The first example of mononuclear isoheterocyclic rearrangement is reported. The 3-benzoylamino-5-methyl-1,2,4-oxadiazole (5) furnishes through a reversible process (slowly at room temperature in methanol, acetone or dioxane, fast in DMSO or in methan
Publikováno v:
Tetrahedron. 30:3859-3864
Publisher Summary This chapter discusses the mononuclear heterocyclic rearrangements. The chapter discusses the ring conversion of type 1→2 characterized by nucleophilic attack from a Z atom on a sp 2 -nitrogen atom with displacement of an atom. On
Publikováno v:
Journal of Heterocyclic Chemistry. 20:931-934
The reaction of 3-benzoyl-5-phenylisoxazole (4) and 3-acetyl-5-methylisoxazole (5) with phenylhydrazine and N-methyl-N-phenylhydrazine has been investigated and the reactivity of (E)- and (Z)-phenylhydrazones and N-methyl-N-phenylhydrazones has been
Publikováno v:
Journal of Heterocyclic Chemistry. 15:1485-1488
The addition reaction of C-acetyl-N-phenylnitrilimine to pyrrole has been investigated. The products obtained show that the reaction proceeds via two distinct pathways. The 1,3-addition reaction leads to the non-cyclic-adduct III, whereas the 1,3-cyc
Polycondensed nitrogen heterocycles. Part21. Complete13C NMR assignment of annelated phenanthridines
Autor:
Werner Hinz, Giuseppe Cusmano, Gaetano Dattolo, Girolamo Cirrincione, And Michele Ruccia, Gabriella Macaluso, And Enrico Aiello, Anna Maria Almerico
Publikováno v:
Journal of Heterocyclic Chemistry. 23:1273-1276
Two-dimensional nmr techniques were used for the complete assignment of 13C nmr spectra of pyrrolo-[1,2-f]-, pyrazolo[1,5-f]-, and 1,2,4-triazolo[1,5-f]phenanthridines.
Publikováno v:
Analytical Biochemistry. 8:512-518
Under mild alkaline conditions hemin can be catalytically hydrogenated to the iron complex of mesoporphyrin IX. Subsequent demetallation yields mesoporphyrin IX. In this way pure mesoporphyrin IX becomes readily accessible. In contrast, the mesoporph
Publikováno v:
Tetrahedron Letters. 13:4703-4706
Publikováno v:
Tetrahedron. 29:3159-3164
The reactivity of indole derivatives towards nitrilimines has been studied. Substituents at positions 1, 2 and 3 of the indole ring greatly affect the course of the reaction. 1,3-Dipolar cycloaddition products (3a,8a,dihydropyrazole-[3,4-b]-indole de
Publikováno v:
J. Chem. Soc., Perkin Trans. 1. :17-19
The behaviour of N-(5-R-1,2,4-oxadiazol-3-yl)-β-enamino ketones towards rearrangement has been investigated. In the presence of anionic reagents in ethanol solution, they rearrange to pyrimidine N-oxides. The synthesis and hydrolytic ring opening of