Výsledky vyhledávání - "Micha Gazowski"

Akademický článek

Oxygenation of alkylzinc complexes with pyrrolylketiminate ligand: access to alkylperoxide versusoxo-encapsulated complexesElectronic supplementary information (ESI) available: Experimental details, 1H NMR spectra and crystal structures of 2and 3showing the cooperative C–Hπ interactions between monomeric units. CCDC numbers 696853–696855. For ESI and crystallographic data in CIF or other electronic format see DOI: 10.1039/b813315hCrystal data for 2: C24H36N4Zn2, M= 511.31, triclinic, a= 8.3637(2) , b= 8.7342(3) , c= 9.4312(3) , α= 105.1357(11)°, β= 104.473(2)°, γ= 104.829(2)°, V= 604.73(3) A3, T= 100(2) K, space group P-1, Z= 1, unique data: 2775, parameters: 172. The final wR(F2) = 0.0563 (all data), CCDC 696853. Crystal data for 3: C40H54N8Zn3O4·toluene, M= 999.22, triclinic, a= 14.6481(3) , b= 18.5359(3) , c= 18.7841(4) , α= 92.2702(10)°, β= 98.1488(10)°, γ= 94.0181(10)°, V= 5029.93(17) A3, T= 100(2) K, space group P-1, Z= 4, unique data: 13 525, parameters: 1130. The final wR(F2) =

Autor: Janusz Lewiski, Karolina Suwaa, Tomasz Kaczorowski, Micha Gazowski, Daniel T. Gryko, Iwona Justyniak, Janusz Lipkowski

Publikováno v: Chemical Communications; Jan2009, Vol. 2009 Issue 2, p215-217, 3p

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