Zobrazeno 1 - 3
of 3
pro vyhledávání: '"Maya Stevenson"'
Autor:
Mark G. Moloney, Stephen J. Heyes, Jonathan E. H. Buston, Timothy D. W. Claridge, Maya Stevenson, Jeremy L. Bretherton
Publikováno v:
Magnetic Resonance in Chemistry. 39:68-76
207Pb NMR spectroscopy was used to investigate 20 lead(IV) tetracarboxylates both in solution and in the solid state by cross-polarization magic angle spinning (CP/MAS) NMR. There is generally good correlation between isotropic chemical shifts in the
Publikováno v:
Inorganic Chemistry. 35:76-81
The reaction of lanthanide triflates with 2 equiv of potassium hydrotris(dimethylpyrazolyl)borate (Tp(Me)()2) gives good yields of complexes of composition Ln(Tp(Me)()2)(2)OTf. For La (2), Ce (3), Pr (4), and Nd (5) the complexes are seven-coordinate
Autor:
Jonathan E. H. Buston, Mark G. Moloney, Keith Prout, Stephen J. Heyes, Michael A. Leech, Maya Stevenson, Timothy D. W. Claridge
Publikováno v:
Dalton Transactions. :3195
A 1 : 1 crystalline complex of lead(IV) tetraacetate and pyridine (LTA-py) has been prepared. The single-crystal X-ray structure, at 296 and 150 K, establishes the presence of a relatively short Pb-N bond (2.307 A) within an intriguing seven-coordina