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pro vyhledávání: '"Matthew J. Jansma"'
Publikováno v:
Nature protocols. 15(7)
An amendment to this paper has been published and can be accessed via a link at the top of the paper.
Autor:
Patrick S. Hanley, Douglas C. Bland, Robert D. J. Froese, Megan A. Cismesia, Matthew J. Jansma, Melanie S. Sanford, Sydonie D. Schimler
Publikováno v:
Journal of the American Chemical Society. 139:1452-1455
This report describes a method for the deoxyfluorination of phenols with sulfuryl fluoride (SO2F2) and tetramethylammonium fluoride (NMe4F) via aryl fluorosulfonate (ArOFs) intermediates. We first demonstrate that the reaction of ArOFs with NMe4F pro
Publikováno v:
Nature Protocols. 15:2277-2277
This protocol is intended to provide chemists who discover or make new organic compounds with a valuable tool for validating the structural assignments of those new chemical entities. Experimental ¹H and/or ¹³C NMR spectral data and its proper int
Publikováno v:
Journal of Natural Products. 75:1326-1331
Phomopsichalasin was isolated and assigned structure 1 over 15 years ago. Analysis of its proton NMR data led us to hypothesize that not all aspects of the relative configuration of this structure were correct. We have used both empirical and computa
Publikováno v:
Nature protocols. 9(3)
This protocol is intended to provide chemists who discover or make new organic compounds with a valuable tool for validating the structural assignments of those new chemical entities. Experimental ¹H and/or ¹³C NMR spectral data and its proper int