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Publikováno v:
Inorganica Chimica Acta. 193:120
Novel square planar methylnickel compounds with benzene-dioxo ligands (OO)[NiMe(PMe3)]2 (O Obenzene-1,2-dioxo (1); benzene-1,2-dioxo-4-methyl (2); benzene-1,2-dioxo-3-methoxo (3)) were prepared from [NiMe(OMe)(PMe3)]2 and the corresponding 1
Autor:
Guy Bertrand, M. Dartiguenave, Marie-J. Menu, Y. Dartiguenave, Antoine Baceiredo, J.J. Bonnet
Publikováno v:
Journal of Organometallic Chemistry. 372:201-206
Crystals of bis[bis(diisopropylamino)phosphanyl]diazomethane P2N6C25H56, M = 502.7 belong to the monoclinic space group, C2/c with a 12.044(2), b 28.661(4) c 10.301(1) A, β 116.13(1)°, V 3192(2) A3 and Z = 4. The structure was refined by use of 127