Výsledky vyhledávání - "Maria Argese"

Solvent-free synthesis of chalcones using Mg(HSO4)2

Autor: Ervis Saraci, Massimiliano Andreoli, Emanuele Casali, Massimo Verzini, Maria Argese, Roberto Fanelli, Giuseppe Zanoni

Publikováno v: RSC Sustainability. 1:504-510

New solvent-free synthesis of relevant chalcones is reported using a simple “endless-screw” reactor, using Mg(HSO4)2 as a catalyst. This shows great promise for industrial use, including to make bioactive drugs like metochalcone and elafibranor.

Externí odkaz: https://explore.openaire.eu/search/publication?articleId=doi_________::7ab4ae321b18d4102bac72974d76de71
https://doi.org/10.1039/d3su00003f

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Process Development and Scale-up of T3-Sulfate, A New Prodrug Alternative to the Conventional Hormone Therapy of Hypothyroidism

Autor: Maria Argese, Sonia Gazzetto, Luciano Lattuada, Valeria Boi, Laura Galimberti

Publikováno v: Organic Process Research & Development. 18:1175-1180

An efficient and scalable preparation of the thyroid hormone analogue O-[3-iodo-4-(sulfooxy)phenyl]-3,5-diiodo-l-tyrosine sodium salt (T3-sulfate, 1) is reported. The synthesis involved monoiodination of O-(4-hydroxyphenyl)-3,5-diiodo-l-tyrosine to g

Externí odkaz: https://explore.openaire.eu/search/publication?articleId=doi_________::21fb4b4cf4e9aee97dcce5859b4ff54a
https://doi.org/10.1021/op500222p

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Synthesis and NMR characterization of cis and trans decahydro-2a,4a,6a,8a-tetraazacyclopent[fg]acenaphthylene. Solid state structure of the trans stereoisomer. Modelling studies

Autor: Mario De Miranda, Paolo Dapporto, Andrea Ferraris, Maria Argese, Patrizia Rossi, Paola Paoli, Marino Brocchetta

Publikováno v: Tetrahedron. 63:6915-6923

The reduction with Vitride® of the cis and trans isomers of octahydro-2a,4a,6a,8a-tetraazacyclopenten[fg]acenaphthylene 1,2-diones (5 and 6) and octahydro-2a,4a,6a,8a-tetraazacyclopenten[fg]acenaphthylene 3,4-diones (7 and 8) led to the cis 9 and th

Externí odkaz: https://explore.openaire.eu/search/publication?articleId=doi_________::a8156323a2dcd14ffe05492e78cee5f4
https://doi.org/10.1016/j.tet.2007.04.036

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Stereochemistry of the intermediates in the synthesis of 1,4,7,10-tetraazacyclododecane from triethylenetetramine, glyoxal and diethyl oxalate

Autor: Marino Brocchetta, Maria Argese, Patrizia Rossi, Mario De Miranda, Fiorenza Perego, Paola Paoli

Publikováno v: Tetrahedron. 62:6855-6861

The equilibrium and rearrangement phenomena encountered in two steps for the synthesis of 1,4,7,10-tetraazacyclododecane from triethylenetetramine, glyoxal and diethyl oxalate were studied and elucidated after the development of two micellar electrok

Externí odkaz: https://explore.openaire.eu/search/publication?articleId=doi_________::a80a52ba90d88ac924e7e951a5aa367c
https://doi.org/10.1016/j.tet.2006.04.099

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