Zobrazeno 1 - 10
of 178
pro vyhledávání: '"MASASHI OHBA"'
Publikováno v:
Chemical Physics. 419:84-89
We have employed a laser desorption technique combined with supersonic-jet cooling for producing base pairs of adenine nucleosides, adenosine (Ado) and N6,N6-dimethyladenosine (DMAdo) under low-temperature conditions. The resulting base pairs are the
Publikováno v:
The Journal of Physical Chemistry A. 114:11231-11237
Monohydration structures of the guanine-guanine and guanine-cytosine base pairs have been elucidated by IR-UV double resonance spectroscopy combined with ab initio calculations. The systems studied consist of the homodimer of 9-methylguanine and the
Autor:
Hitomi Tada, Tomoko Ohkubo, Yutaro Miyamoto, Yasuhito Kobayashi, Yasutaka Tajima, Masashi Ohba, Kazuo Yamazaki
Publikováno v:
HETEROCYCLES. 96:324
Autor:
Itaru Natsutani, Masashi Ohba
Publikováno v:
Tetrahedron. 63:12689-12694
A full account of the total synthesis of 18-demethyl-19-hydroxy-Na-demethyl-Nb-methylsuaveoline (1), the structure assigned to macrocaffrine isolated from Rauwolfia caffra, is presented. The key steps involved are an intramolecular cycloaddition reac
Publikováno v:
Tetrahedron. 63:10337-10344
A full account of the highly stereoselective total synthesis of two indole alkaloids, suaveoline ( 4 ) and norsuaveoline ( 5 ), is presented. Central features of the synthetic strategy include the conversion of l -tryptophan methyl ester ( 12 ) into
Autor:
Masashi Ohba, Kei Fukuyama, Aiko Hosoi, Kazuyoshi Takeda, Akihiro Nishibayashi, Yoshinori Okuno, Shigeki Isomura
Publikováno v:
ChemInform. 46
2,4,6-Trichlorobenzoyl-4-dimethylaminopyridine (modified Yamaguchi reagent) is shown to be an efficient reagent for the esterification, that allows to avoid the use of intractable acid chlorides as well as acid anhydrides.
Publikováno v:
Chemical and Pharmaceutical Bulletin. 54(1):63-67
A full account of the total synthesis of two monoterpene alkaloids, (-)-plectrodorine [(-)-1] and (+)-oxerine [(+)-3], is presented. The key steps involved are the formation of the oxazole alcohol 10 from the γ-butyrolactone 9 and the intramolecular
Publikováno v:
Tetrahedron Letters. 45:6471-6474
Total synthesis of two Rauwolfia alkaloids, suaveoline ( 1 ) and norsuaveoline ( 2 ), has been achieved through a highly stereoselective route starting from l -tryptophan methyl ester ( 9 ) and exploiting the intramolecular Diels–Alder reaction of
Autor:
Masashi Ohba, Itaru Natsutani
Publikováno v:
Heterocycles. 63(12):2845-2850
A synthesis of Na-demethyl-20-deethylsuaveoline (1), the structure assigned to the Rauwolfia alkaloid sellowiine, has been accomplished for the first time through a route using intramolecular oxazole-olefin Diels-Alder reaction. The 1 H- and 1 3 C-NM
Autor:
Keisuke Uji, Midori Tabata, Keitaro Suzuki, Kazuaki Ohyama, Sachiko Yanagihara, Kazuo Yamazaki, Tetsuji Hosono, Ai Tatara, Mai Aritake, Shungo Takamoto, Kei Ogiso, Masashi Ohba, Takumi Sugahara
Publikováno v:
HETEROCYCLES. 94:503