Zobrazeno 1 - 10
of 23
pro vyhledávání: '"M. Tereza Fernandez"'
Autor:
Vitor Pinto, M. Filomena Duarte, Paula Rodrigues, M. Teresa Barros, G. John Langley, Benedito J. Costa Cabral, M. Tereza Fernandez, M. Lourdes Costa, Susana C. R. Marques, Narciso Couto
Publikováno v:
Rapid Communications in Mass Spectrometry. 31:1001-1013
RATIONALE The complexation behavior of transition metals with organic azides by electrospray ionization (ESI) tandem mass spectrometry (MS/MS) is not completely understood. In this study, fragmentation patterns of complex ions having azidoacetic acid
Autor:
M. Filomena Duarte, Benedito J. Costa Cabral, Ana Assis, M. Tereza Fernandez, Paula Rodrigues, M. Lourdes Costa, M. Teresa Barros, Narciso Couto
Publikováno v:
Journal of Mass Spectrometry. 46:696-704
The relevance of metal interactions with azides has led us to the study of the complexation of some transition metals, nickel and cobalt, by azidoacetone by means of electrospray ionization mass spectrometry (ESI-MS). Complexes were obtained from sol
Autor:
M. Filomena Duarte, Narciso Couto, Paula Rodrigues, Benedito J. Costa Cabral, M. Lourdes Costa, M. João Ramos, M. Teresa Barros, M. Tereza Fernandez
Publikováno v:
Rapid Communications in Mass Spectrometry. 22:582-590
The present work describes a study of the complexation of calcium and magnesium by 3-azidopropionitrile by means of electrospray ionization mass spectrometry (ESI-MS). Complexes were obtained from solutions of calcium and magnesium salts of the type
Autor:
Paula Rodrigues, M. Filomena Duarte, M. Tereza Fernandez, Benedito J. Costa Cabral, M. Lourdes Costa, Narciso Couto, M. Teresa Barros
Publikováno v:
Journal of the American Society for Mass Spectrometry. 18:453-465
Most complexes of azides and transition metals involve the N(3)(-) azide anion as a ligand other than an organic azide. Complexes of organic azides with metals are involved in biological applications and in the deposition of nitrenes on metal surface
Publikováno v:
Rapid Communications in Mass Spectrometry. 20:2309-2316
Electron ionisation mass spectrometry studies were performed previously for p-diphenyl carbonate and some monosubstituted diphenyl carbonates. In this work, p-diphenyl carbonate and p-methoxyphenylphenyl carbonate are re-examined, and p-chlorophenyl
Autor:
Filipa M. S. Martins, M. Lourdes Costa, G. John Langley, M. Filomena Duarte, M. Teresa Barros, M. Tereza Fernandez, Paula Rodrigues
Publikováno v:
Rapid Communications in Mass Spectrometry. 17:957-962
A series of derivatives of 2-azidoacetic acid and 2-azidoacetone were synthesized and their behaviour under electron ionization conditions was investigated. This paper reports the electron ionization fragmentation mechanisms for five aliphatic α-car
Autor:
Andrew C. Gill, Keith R. Jennings, Lurdes Mira, M. Helena Florêncio, M. Tereza Fernandez, Manuela Silva
Publikováno v:
Journal of Inorganic Biochemistry. 71:93-98
Captopril, enalaprilat and lisinopril, angiotensin-converting enzyme (ACE) inhibitors, are effective HO • radical scavengers and seem to have some degree of metal binding capabilities. By metal chelation iron and copper may become inactive in radic
Publikováno v:
Journal of the Chemical Society, Faraday Transactions. 94:1427-1430
Gas-phase basicity (GB) and proton affinity (PA) of limonene were derived from measurements of proton transfer equilibria carried out by high pressure pulsed electron beam source mass spectrometry. Experimental GB and PA are 842±5 kJ mol-1 and 875±
Publikováno v:
Journal of the Chemical Society, Perkin Transactions 2. :873-880
Gas phase proton transfer equilibria involving ortho-, meta- and para-isomers of tolualdehyde, fluorobenzaldehyde and chlorobenzaldehyde have been studied experimentally for the first time as a function of temperature. Proton affinities have been det
Publikováno v:
Rapid Communications in Mass Spectrometry. 8:187-194
Cathodic ion sputtering energies have been studied in a glow-discharge ion source, operated in the ranges 0.5–2.0 Torr pressure and 100–1000 V discharge voltage using ion kinetic energy spectroscopy. Average energies in the range 10–20 eV were