Zobrazeno 1 - 10
of 17
pro vyhledávání: '"M. M. Delgado Zamarreño"'
Publikováno v:
Analytica Chimica Acta. 386:99-106
An automated procedure for the determination of vitamin E in samples of butter with minimum sample manipulation has been developed. Following dissolution of the samples in a micellar medium (methanol–Triton X-100–water), on-line sample treatment
Publikováno v:
The Analyst. 120:139-142
Casein greatly reduces the overvoltage for the polarographic reduction of NiII in sodium acetate medium. Using polarographic chronoamperometry, current–time curves were obtained from which the electrocatalytic effect of casein could be evaluated. T
Autor:
J. Hernandez Mendez, A. Sanchez Perez, M. C. Gomez Perez, M. A. Fernandez Moro, M. M. Delgado Zamarreño
Publikováno v:
The Analyst. 120:2489-2492
A high-performance liquid chromatographic method with dual-electrochemical detection (HPLC-DEC) for the simultaneous determination of vitamins A, E and K1 is described. Separation was carried out using a C18 reversed-phase column and 2.5 mmol l-1 ace
Publikováno v:
Analytical Letters. 26:2565-2573
The electrochemical behaviour of vitamin D3 and 25-hydroxyvitamin D3 (25-OH D3) in a high performance liquid chromatography system using amperometric detection is described. Separation is carried out using a C18 reversed-phase column and the optimum
Publikováno v:
Journal of chromatography. A. 871(1-2)
Capillary electrokinetic chromatography is suitable for the separation of mixtures of uncharged and charged solutes. In the present work the behavior of six synthetic food antioxidants--2[3]-tert.-butyl-4-hydroxyanisole, 2,6-di-tert.-butyl-p-cresol,
Autor:
J. Hernández Méndez, M. Sanchez Rodriguez, A. Sanchez Perez, M. C. Gomez Perez, M. M. Delgado Zamarreño
Publikováno v:
Talanta. 43(9)
A method employing HPLC with electrochemical detection for the rapid and simultaneous determination of vitamins A, D3 and E is described. The method uses a C-18 reverse phase column and 2.5 mM HAcO-NaAcO in methanol-water (99:1, v/v) solution as the
Publikováno v:
Journal of chromatography. 623(1)
A high-performance liquid chromatographic electrochemical detection for the rapid and simultaneous determination of the vitamin A, D3 and E is described. The separation is carried out by using a C18 reversed-phase column and 0.1 M LiClO4 in methanol-
Publikováno v:
Journal of Pharmaceutical and Biomedical Analysis. 7:1213-1216
The present paper described the voltammetric behaviour of 25-OH D 3 as a means for determining the substance at low concentrations. The new method may be applied to the electroanalytical determination of 25-OH D 3 in samples of pharmaceutical interes
Publikováno v:
Analytica Chimica Acta. 160:335-340
A nickel-catalytic pre-peak at −0.72 V vs. Ag/AgCl, is caused by cephalexin in sodium acetate (pH 8.3) medium. It is used to determine 2.4 × 10−7–6 × 10−6 M cephalexin; the relative standard deviation is 4% for 0.88 μg ml−1 cephalexin. O
Publikováno v:
Analytica Chimica Acta. 176:279-284
In the polarographic reduction of ranitidine, an H2-antagonist of histamine, three waves are observed; their half-wave potentials and limiting currents depend strongly on the pH of the solution. The first and second waves are due to reduction of teh