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pro vyhledávání: '"Luche reduction"'
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Akademický článek
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Publikováno v:
The Journal of Organic Chemistry. 86:13572-13582
A full account of our efforts toward the stereoselective total synthesis of sesquiterpenoid-derived natural products (±)-pleurospiroketals A and B is described. Commercially available 3-methyl-2-cyclohexenone and 2,2-dimethyloxirane were used as key
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_dedup___::ecfd2047afda5c15c4aad21fdd7487c2
https://doi.org/10.1021/acs.joc.1c01634
https://doi.org/10.1021/acs.joc.1c01634
Autor:
Philipp Fruhmann, Christian Hametner, Hannes Mikula, Gerhard Adam, Rudolf Krska, Johannes Fröhlich
Publikováno v:
Toxins, Vol 6, Iss 1, Pp 325-336 (2014)
The trichothecene mycotoxin deoxynivalenol (DON) is a well known and common contaminant in food and feed. Acetylated derivatives and other biosynthetic precursors can occur together with the main toxin. A key biosynthetic step towards DON involves an
Externí odkaz:
https://doaj.org/article/79543f022deb4001b3021a786496effb
Publikováno v:
European Journal of Organic Chemistry. 2021:1156-1167
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::a3a3c40fbcb1ec36416430687b9b5988
https://doi.org/10.1002/ejoc.202001591
https://doi.org/10.1002/ejoc.202001591
Autor:
Song Qiuling, Wenxue Wu, Jie Yan, Shinya Iimura, Mark S. Bednarz, Dai Kuangchu, Matthew Mangzhu Zhao, Haiming Zhang, Xiaodong Gu, Youchu Wang, Ngiap-Kie Lim
Publikováno v:
Organic Process Research & Development. 24:2689-2701
The development of an efficient manufacturing process for sotagliflozin (LX4211), a dual inhibitor of sodium–glucose cotransporter-1/2 (SGLT-1/2) for the treatment of diabetes, is described. Sotagl...
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::3c3755ff6820ddf3fa9552ad3ec4a108
https://doi.org/10.1021/acs.oprd.0c00359
https://doi.org/10.1021/acs.oprd.0c00359
Autor:
Philemon Ngoje, David Crich
Publikováno v:
Org Lett
We describe the synthesis of the unusual bicyclic sugar bradyrhizose in 14 steps and a 6% overall yield from d-glucose. The synthesis involves the elaboration of a trans-fused carbocyclic ring onto the preexisting glucopyranose framework followed by
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_dedup___::a57fa76c79e593f30134663136ed8b35
https://doi.org/10.1021/acs.orglett.9b04279
https://doi.org/10.1021/acs.orglett.9b04279
Cerium(III) Chloride-Mediated Stereoselective Reduction of a 4-Substituted Cyclohexanone Using NaBH4
Autor:
Martin D. Eastgate, Ian S. Young, Manjunath Gujjar, Prantik Maity, Raghukumar Vellingiri, Thirumalai Lakshminarasimhan, Rajappa Vaidyanathan, Albert J. DelMonte
Publikováno v:
Organic Process Research & Development. 23:2754-2757
Several additives were screened for the stereoselective reduction of a 4-substituted cyclohexanone en route to linrodostat mesylate. It was found that the addition of sub-stoichiometric cerium(III)...
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::20ca37362328582ba594dac236a1411f
https://doi.org/10.1021/acs.oprd.9b00458
https://doi.org/10.1021/acs.oprd.9b00458
Akademický článek
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Publikováno v:
Reaction Kinetics, Mechanisms and Catalysis. 125:47-53
The Noyori-type (1S,2S)- and (1R,2R)-N-(para-tosyl)-1,2-diphenylethylene-1,2-diamine ligands complexed with ruthenium have been found to be effective catalysts for the regiospecific transfer hydrogenation of 3-methoxy- and 3-benzyloxy-(Z)16-hydroxyme
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::73ef42b4b1c8db3f96911b03b299cce8
https://doi.org/10.1007/s11144-018-1453-6
https://doi.org/10.1007/s11144-018-1453-6