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pro vyhledávání: '"Leszek Łuczak"'
Publikováno v:
Heteroatom Chemistry. 6:365-370
An efficient procedure is described that leads to pure (SP)-O-l-menthylphenylthiophosphinate. The absolute configuration of this diastereomer was assigned by chemical correlation and confirmed by X-ray crystallography. The reaction of the isomer with
Publikováno v:
Phosphorus, Sulfur, and Silicon and the Related Elements. 95:371-374
Stereoselective synthesis of the P-chiral thioxaphosphoranesulfenyl (dicyclohexyl)amide (l-menthyl-O)PhP(S)SN(C6H11)2 and its conversion into the P-chiral thioxaphosphoranesulfenyl chloride (l-menthyl-O)PhP(S)SCl is described. First synthesis of P-ch
Publikováno v:
Tetrahedron. 37:2011-2020
Optically active t-butylphenylphosphinothiocyanidate Bu t PhP(O)SCN 3 and t-butyl-O-methyl-phosphonothiocyanidate Bu t (MeO)P(O)SCN 7 have been prepared by condensation of the corresponding sulphenyl chlorides > P(O)SCl with trimethylsilylcyanide and
Publikováno v:
Phosphorous and Sulfur and the Related Elements. 40:233-236
Dialkylthioxaphosphoranesulfenyl chlorides and bromides can be conveniently prepared in the reaction of the corresponding thioamides with hydrogen chloride generated in situ with trimethylsilyl chloride and ethanol. Stability of the chlorides and bro