Zobrazeno 1 - 10
of 93
pro vyhledávání: '"Leslie H. Sutcliffe"'
Autor:
Leslie H. Sutcliffe, Shirley A. Fairhurst, Keith F. Preston, Yuen-Li Chung, Duncan G. Gillies
Publikováno v:
Magnetic Resonance in Chemistry. 30:666-672
Further information has been obtained on the electronic structure of 1,3,2-dithiazol-2-yl radicals. The structure has been well characterized previously except for positions 4 and 5 in the ring. We have obtained solution and powder ESR spectra of rad
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::d78b9f6290fdf446346d61f922c3bc73
https://doi.org/10.1002/mrc.1260300717
https://doi.org/10.1002/mrc.1260300717
Publikováno v:
Magnetic Resonance in Chemistry. 43:457-462
The spin probes 1,1,3,3-tetramethylisoindolin-2-yloxyl (TMIO) and the sodium salt of its sulfonate, 1,1,3,3-tetramethylisoindolin-2-yloxyl-5-sulfonate (NaTMIOS) were used to monitor the microviscosity changes of water during starch gelatinization. In
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_dedup___::a4d729c5ab4bf6741dfad7c82c74a6f5
https://doi.org/10.1002/mrc.1567
https://doi.org/10.1002/mrc.1567
Publikováno v:
Magnetic Resonance in Chemistry. 40:57-64
Cobalt-59 NMR measurements were made on an aqueous solution of K3[Co(CN)6] with pressure as the main variable. We determined the effect of temperature and pressure (up to 5 kbar) on (i) the cobalt-59 chemical shift, (ii) the carbon–cobalt-59 isotop
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::9a34cab6eff4373bfeaaab21bc2eb054
https://doi.org/10.1002/mrc.955
https://doi.org/10.1002/mrc.955
Autor:
Leslie H. Sutcliffe, Steven E. Bottle, David L. Hughes, Duncan G. Gillies, Alex I. Smirnov, Aaron S. Micallef
Publikováno v:
Journal of the Chemical Society, Perkin Transactions 2. :1285-1291
Here we describe the improved synthesis and full characterisation, including W-band EPR analysis and X-ray crystallography, of an anionic isoindoline aminoxyl, 5-carboxy-1,1,3,3-tetramethylisoindolin-2-yloxyl 6 (CTMIO), which is more water soluble th
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::f52a4cf459b6f890627f930f16a3eb45
https://doi.org/10.1039/b002497j
https://doi.org/10.1039/b002497j
Autor:
Scott Brownridge, Shirley A. Fairhurst, Simon Parsons, Nicholas P. C. Westwood, Melbourne J. Schriver, Hongbin Du, Leslie H. Sutcliffe, Robert C. Haddon, Heinz Oberhammer, Jack Passmore
Publikováno v:
Journal of the Chemical Society, Dalton Transactions. :3365-3382
The first structural characterisation of a heterocyclic free radical in all phases has been achieved. 4,5-Bis(trifluoromethyl)-1,3,2-dithiazol-2-yl, [CF3CSNSCCF3]˙ 4d, a 7π radical, was prepared quantitatively on reduction of [4d][AsF6] with variou
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::c2cf34893761c3dcd6bd05905028ee32
https://doi.org/10.1039/b001489n
https://doi.org/10.1039/b001489n
Publikováno v:
Journal of Agricultural and Food Chemistry. 47:4520-4524
New water-soluble and lipid-soluble spin probes suitable for the ESR investigation of the physical states and interactions of components of dough have been developed. This paper reports some preliminary findings on the suitability of these probes for
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_dedup___::61a9405c44f7853168eeb78ffd54a4b8
https://doi.org/10.1021/jf981385w
https://doi.org/10.1021/jf981385w
Publikováno v:
Magnetic Resonance in Chemistry. 37:730-734
The stable free radical 1,1,3,3-tetramethylisoindolin-2-yloxyl (TMIO) has proved to be very suitable for use as a spin probe for a number of applications. Because it is soluble mainly in non-polar liquids, there is a need for new derivatives that can
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::783764916bbde645d4e233478b363e12
https://doi.org/10.1002/(sici)1097-458x(199910)37:10<730::aid-mrc530>3.0.co
https://doi.org/10.1002/(sici)1097-458x(199910)37:10<730::aid-mrc530>3.0.co
Publikováno v:
Magnetic Resonance in Chemistry. 37:36-42
A new ESR spin probe, sodium 1,1,3,3-tetrakis(trideuteromethyl)isoindolin-2- yloxyl-4-sulphonate, which is related to the extensively studied generic free radical 1,1,3,3-tetramethylisoindolin-2-yloxyl (TMIO), was synthesized. The latter has greater
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::5ade1b076de219d15ae5638da4e87a1e
https://doi.org/10.1002/(sici)1097-458x(199901)37:1<36::aid-mrc405>3.0.co
https://doi.org/10.1002/(sici)1097-458x(199901)37:1<36::aid-mrc405>3.0.co
Autor:
Alex I. Smirnov, Melanie M. Britton, Duncan G. Gillies, Susan A. Fawthrop, Leslie H. Sutcliffe, Xiaoping Wu
Publikováno v:
Magnetic Resonance in Chemistry. 35:493-501
For ESR studies of molecular rotation in liquids, it is desirable to match the spin probe as closely as possible to the solvent molecules. In this work the solvents were model lubricants whose overall motion has been characterized from carbon-13 NMR
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::c392fd9fafc622dfc0c724eaaec97b42
https://doi.org/10.1002/(sici)1097-458x(199708)35:8<493::aid-omr121>3.0.co
https://doi.org/10.1002/(sici)1097-458x(199708)35:8<493::aid-omr121>3.0.co
Autor:
C.R. Baldwin, Glen W. Smith, Melanie M. Britton, D.L. Hughes, Leslie H. Sutcliffe, Duncan G. Gillies, S.C. Davies
Publikováno v:
Journal of Molecular Structure. 403:1-16
The X-ray structures and proton and carbon-13 NMR spectra have been obtained for two dicyclohexyl esters and one tricyclohexyl ester: namely, di-2-methylcyclohexylsuccinate (D2MCS), dicyclohexyl-3,4-furandicarboxylate (DCFDC) and tricyclohexyl-1,2,3-
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::938420452d6c3fa89b4df943867a88f0
https://doi.org/10.1016/s0022-2860(96)09413-6
https://doi.org/10.1016/s0022-2860(96)09413-6