Multiresidue Determination of Growth Promoters in Bovine Serum using QuEChERS and UHPLC-Q-ORBITRAP: Validation and In Vivo Study.

Autor: da Silva MC; Departamento de Química, Instituto de Ciências Exatas - Universidade Federal de Minas Gerais, Av. Antônio Carlos, 6627, Belo Horizonte, MG 31270-901, Brazil., Rocha DG; Departamento de Química, Instituto de Ciências Exatas e Biológicas - Universidade Federal de Ouro Preto. Campus Morro do Cruzeiro, Ouro Preto, MG 35400-000, Brazil., Lana MAG; Laboratório Federal de Defesa Agropecuária de Minas Gerais - Ministério da Agricultura e Pecuária - Brazil, Av. Rômulo Joviano, Pedro Leopoldo, MG 33250-220, Brazil., de Assis DCS; Escola de Veterinária, Universidade Federal de Minas Gerais, Av. Antônio Carlos, 6627, Belo Horizonte, MG 30123-970, Brazil., Pereira MPM; Escola de Veterinária, Universidade Federal de Minas Gerais, Av. Antônio Carlos, 6627, Belo Horizonte, MG 30123-970, Brazil., Faria AF; Departamento de Química, Instituto de Ciências Exatas - Universidade Federal de Minas Gerais, Av. Antônio Carlos, 6627, Belo Horizonte, MG 31270-901, Brazil.

Publikováno v: Journal of agricultural and food chemistry [J Agric Food Chem] 2023 Oct 25; Vol. 71 (42), pp. 15766-15773. Date of Electronic Publication: 2023 Oct 16.

Critical Evaluation of Two Qualitative Analytical Approaches for Multiclass Determination of Veterinary Drugs in Bovine Muscle Using UHPLC-Q-Orbitrap: The Wind of Change in Brazilian Monitoring.

Autor: Paula RAO; Postgraduate Program in Food Science, Department of Food Science (ALM), Faculty of Pharmacy (FAFAR), Federal University of Minas Gerais (UFMG), Campus da UFMG, Antônio Carlos Avenue 6627, Belo Horizonte 31270-010, Brazil., Gondim CS; Postgraduate Program in Food Science, Department of Food Science (ALM), Faculty of Pharmacy (FAFAR), Federal University of Minas Gerais (UFMG), Campus da UFMG, Antônio Carlos Avenue 6627, Belo Horizonte 31270-010, Brazil., Schmidt EM; Nova Analítica Importações e Exportações LTDA, Assungui Street, 432, Vila Gumercindo, São Paulo 04131-000, Brazil., Diniz MHGM; Food of the Agricultural Defense Federal Laboratory of Minas Gerais, Ministry of Agriculture and Livestock, Rômulo Joviano Avenue, s/nº, Centro, Pedro Leopoldo 33600-000, Brazil., Lana MAG; Food of the Agricultural Defense Federal Laboratory of Minas Gerais, Ministry of Agriculture and Livestock, Rômulo Joviano Avenue, s/nº, Centro, Pedro Leopoldo 33600-000, Brazil., Oliveira LS; Postgraduate Program in Food Science, Department of Food Science (ALM), Faculty of Pharmacy (FAFAR), Federal University of Minas Gerais (UFMG), Campus da UFMG, Antônio Carlos Avenue 6627, Belo Horizonte 31270-010, Brazil.; Department of Mechanical Engineering, Engineering School, Federal University of Minas Gerais (UFMG), Campus da UFMG, Antônio Carlos Avenue 6627, Belo Horizonte 31270-010, Brazil.

Publikováno v: Molecules (Basel, Switzerland) [Molecules] 2023 May 17; Vol. 28 (10). Date of Electronic Publication: 2023 May 17.

A novel strategy for the detection of boldenone undecylenate misuse in cattle using ultra-high performance liquid chromatography coupled to high resolution orbitrap mass spectrometry: From non-targeted to targeted.

Autor: Rocha DG; Department of Chemistry-Institute of Exact Sciences, Federal University of Minas Gerais, Belo Horizonte, Brazil.; Federal Laboratory of Animal and Plant Health and Inspection-Ministry of Agriculture, Livestock and Food Supply, Pedro Leopoldo, Brazil., Lana MAG; Federal Laboratory of Animal and Plant Health and Inspection-Ministry of Agriculture, Livestock and Food Supply, Pedro Leopoldo, Brazil., de Assis DCS; Veterinary School, Federal University of Minas Gerais, Belo Horizonte, Brazil., de Macedo AN; Department of Chemistry-Institute of Exact Sciences, Federal University of Minas Gerais, Belo Horizonte, Brazil., Corrêa JMM; Department of Chemistry-Institute of Exact Sciences, Federal University of Minas Gerais, Belo Horizonte, Brazil., Augusti R; Department of Chemistry-Institute of Exact Sciences, Federal University of Minas Gerais, Belo Horizonte, Brazil., Faria AF; Department of Chemistry-Institute of Exact Sciences, Federal University of Minas Gerais, Belo Horizonte, Brazil.

Publikováno v: Drug testing and analysis [Drug Test Anal] 2022 Apr; Vol. 14 (4), pp. 667-675. Date of Electronic Publication: 2021 Dec 20.

Can Serum be a Match for Urine in the Regulatory Analysis of Boldenone in Cattle? A Systematic Comparison Between Detection Window, Stability, and Enzymatic Hydrolysis.

Autor: Rocha DG; Department of Chemistry-Institute of Exact Sciences, Federal University of Minas Gerais, Av. Antônio Carlos 6627, Belo Horizonte, MG31270-901, Brazil.; Federal Laboratory of Animal and Plant Health and Inspection, Ministry of Agriculture, Livestock and Food Supply, Av. Rômulo Joviano s/n, Pedro Leopoldo, MG 33600-000, Brazil., Lana MAG; Federal Laboratory of Animal and Plant Health and Inspection, Ministry of Agriculture, Livestock and Food Supply, Av. Rômulo Joviano s/n, Pedro Leopoldo, MG 33600-000, Brazil., Dracz S; Federal Laboratory of Animal and Plant Health and Inspection, Ministry of Agriculture, Livestock and Food Supply, Av. Rômulo Joviano s/n, Pedro Leopoldo, MG 33600-000, Brazil., da Silva RR; Federal Laboratory of Animal and Plant Health and Inspection, Ministry of Agriculture, Livestock and Food Supply, Av. Rômulo Joviano s/n, Pedro Leopoldo, MG 33600-000, Brazil., de Assis DCS; Veterinary School, Federal University of Minas Gerais, Av. Antônio Carlos 6627, Belo Horizonte, MG 30123-970, Brazil., da Silva MC; Department of Chemistry-Institute of Exact Sciences, Federal University of Minas Gerais, Av. Antônio Carlos 6627, Belo Horizonte, MG31270-901, Brazil., Augusti R; Department of Chemistry-Institute of Exact Sciences, Federal University of Minas Gerais, Av. Antônio Carlos 6627, Belo Horizonte, MG31270-901, Brazil., Faria AF; Department of Chemistry-Institute of Exact Sciences, Federal University of Minas Gerais, Av. Antônio Carlos 6627, Belo Horizonte, MG31270-901, Brazil.

Publikováno v: Journal of agricultural and food chemistry [J Agric Food Chem] 2021 May 19; Vol. 69 (19), pp. 5528-5535. Date of Electronic Publication: 2021 May 10.

Determination of steroids in bovine hair: Validation of a microwave-assisted chemical derivatization method using liquid chromatography-tandem mass spectrometry and in vivo studies.

Autor: Rocha DG; Department of Chemistry, Institute of Exact Sciences, Federal University of Minas Gerais, Belo Horizonte, MG, Brazil.; Federal Laboratory of Animal and Plant Health and Inspection, Ministry of Agriculture, Livestock and Food Supply, Pedro Leopoldo, MG, Brazil., Lana MAG; Federal Laboratory of Animal and Plant Health and Inspection, Ministry of Agriculture, Livestock and Food Supply, Pedro Leopoldo, MG, Brazil., de Assis DCS; Veterinary School, Federal University of Minas Gerais, Belo Horizonte, MG, Brazil., Cançado SV; Veterinary School, Federal University of Minas Gerais, Belo Horizonte, MG, Brazil., Augusti R; Department of Chemistry, Institute of Exact Sciences, Federal University of Minas Gerais, Belo Horizonte, MG, Brazil., Faria AF; Department of Chemistry, Institute of Exact Sciences, Federal University of Minas Gerais, Belo Horizonte, MG, Brazil.

Publikováno v: Drug testing and analysis [Drug Test Anal] 2020 Aug; Vol. 12 (8), pp. 1078-1086. Date of Electronic Publication: 2020 Jun 30.