Zobrazeno 1 - 10
of 14
pro vyhledávání: '"L. V. Usova"'
Autor:
L. V. Usova, Yu. G. Lavrent'ev
Publikováno v:
Russian Geology and Geophysics. 62:1209-1213
—The basic software package of a JXA-8230 microanalyzer, like its predecessor JXA-8100, uses the long-established ZAF correction method (with some differences) for a quantitative analysis: Calculation of mass absorption coefficients is based on Cha
Publikováno v:
Journal of Analytical Chemistry. 75:902-908
To increase the accuracy of electron probe microanalysis, it was proposed to calculate absorption coefficients range-by-range, with selecting an optimum calculation method for each absorption range. The approach was implemented in the analysis of roc
Autor:
L. V. Usova, Yu. G. Lavrent'ev
Publikováno v:
Russian Geology and Geophysics. 59:1461-1468
X-ray electron probe microanalysis is a complete mineral analysis technique. Therefore, the sum of obtained concentrations can be used as an indicator of the quality of analysis. There are two kinds of errors of the sum of concentrations. The first i
Autor:
Yu. G. Lavrent'ev, L. V. Usova
Publikováno v:
Journal of Analytical Chemistry. 73:42-49
Four methods of correction and three methods of calculation of absorption coefficients are tested in electron probe microanalysis of rock-forming minerals. Experimental data by Pouchou and Pichoir, Sewell–Love–Scott, and Armstrong are attracted i
Autor:
L. V. Usova, Yu. G. Lavrent’ev
Publikováno v:
Аналитика и контроль. 20:15-22
Publikováno v:
Russian Geology and Geophysics. 56:1428-1436
The protocol for analysis of rock-forming mineral compositions by X-ray electron probe microanalysis used at the Institute of Geology and Mineralogy, Novosibirsk, Russia, is described. The analysis is conducted with a JXA-8100 electron probe microana
Publikováno v:
Russian Geology and Geophysics. 56:1154-1161
The results of electron probe microanalysis of several rock-forming minerals by wavelength-dispersive spectrometry (WDS) and energy-dispersive spectrometry (EDS) are compared, and the metrological characteristics of both methods are studied. The meas
Publikováno v:
Journal of Analytical Chemistry. 66:831-837
Crystals of 15 rare-earth element phosphates, which provide a set of standard reference samples in X-ray electron probe microanalysis, were synthesized and tested for homogeneity and stoichiometry. The phosphates were synthesized in two stages, the p
Autor:
Alexey Ragozin, N. S. Karmanov, L. V. Usova, Nikolay V. Sobolev, Alla M. Logvinova, O. A. Kozmenko, Yu. G. Lavrent'ev
Publikováno v:
Doklady Earth Sciences. 439:970-973
Publikováno v:
Journal of Analytical Chemistry. 65:249-254
Specific sources of measurement errors have been studied. In the presence of perturbing radiation, the automatic setting of the spectrometer discrimination mode is not reasonable. When choosing the transmittance window, the dependence of the shift of