Zobrazeno 1 - 10
of 30
pro vyhledávání: '"L. S. Gorshkova"'
Autor:
Marina I. Struchkova, V. A. Ferapontov, L. S. Gorshkova, O. V. Turova, Maxim G. Vinogradov, E. V. Starodubtseva
Publikováno v:
Tetrahedron. 64:11713-11717
A convenient one-step synthesis of chiral γ-lactones has been performed. The method is based on enantioselective hydrogenation of γ-ketoesters using the RuCl 3 –BINAP–HCl catalytic system. Chiral γ-lactones (91–99% ee) have been isolated in
Publikováno v:
Russian Chemical Bulletin. 54:2374-2378
The rate of hydrogenation of γ-ketoesters MeCOCH2CH2COOR (R = Et, Pri, But) in the presence of the chiral RuII—BINAP catalyst (BINAP is 2,2′-bis(diphenylphosphino)-1,1′-binaphthyl) greatly increases upon the addition of 5–10 equivalents of H
Autor:
G. V. Chel'tsova, G. L. Heise, V. A. Ferapontov, D. V. Kurilov, O. V. Shishk, Maxim G. Vinogradov, L. S. Gorshkova
Publikováno v:
Russian Chemical Bulletin. 52:1841-1846
An improved procedure was developed for asymmetric reduction of acetophenone and propiophenone by the chiral reagent NaAl(IPTOLate)H2. This procedure is based on isolation of the chiral alcohol that formed as a crystalline host—guest complex with t
Autor:
G. L. Heise, V. A. Ferapontov, L. S. Gorshkova, I. V. Razmanov, V. A. Pavlov, Maxim G. Vinogradov, G. V. Chel\\'tsova, O. R. Malyshev
Publikováno v:
Russian Chemical Bulletin. 52:471-479
Prochiral substrates (alkyl aryl ketones, cyclopropyl methyl ketone, 1-indanone, 1-tetralone, ethyl 2-oxo-4-phenylbutyrate, and N-(diphenylphosphinyl)acetophenoneimine) were subjected to asymmetric reduction with aluminum hydride reagents, which were
Autor:
G. V. Chel'tsova, L. S. Gorshkova, I. V. Razmanov, V. A. Ferapontov, O. R. Malyshev, M. G. Vinogradov, O. V. Mikhalev, G. L. Heise, V. A. Pavlov
Publikováno v:
Russian Chemical Bulletin. 49:460-465
New stereoselective reducing reagents were preparedin situ by modification of NaAlH4 with various chiral diols. The efficiency of 1,4- and 1,3-diols as chiral auxiliaries in the reactions of alkyl aryl ketones with modified NaAlH4 was considerably hi
Publikováno v:
Russian Chemical Bulletin. 56:552-554
A comparative study of asymmetric hydrogenation and deuteration of methyl levulinate catalyzed by the RuII—(S)-BINAP—HCl system (BINAP is 2,2′-bis(diphenylphosphino)-1,1′-binaphthyl) in MeOH and MeOD was carried out. The results obtained sugg
Autor:
L. N. Kalgorodova, G. I. Nikishin, Maxim G. Vinogradov, A. V. Ignatenko, E. K. Starostin, G. V. Chel'tsova-Bebutova, L. S. Gorshkova, E. A. Shapiro
Publikováno v:
Russian Chemical Bulletin. 44:167-171
A convenient preparative synthesis of cilastatin, an inhibitor of renal dipeptidase used in drugs with the antibiotic imipenem, has been elaborated. The key intermediate in this synthesis is 2-amino-7-chloroheptanoic acid prepared by oxidative cleava
Autor:
K. N. Gavrilov, E. I. Klabunovskii, V. A. Pavlov, E. E. Nifant'ev, E. Yu. Zhorov, L. S. Gorshkova, A. T. Teleshev
Publikováno v:
ChemInform. 23
Autor:
E. A. Mistryukov, L. S. Gorshkova, Dmitry N. Platonov, O. A. Fedotova, V. A. Pavlov, V. I. Shvedov, E. I. Klabunovskii, E. Yu. Zhorov
Publikováno v:
ChemInform. 23
Publikováno v:
ChemInform. 26