Zobrazeno 1 - 10
of 13
pro vyhledávání: '"L. E. Mikhailov"'
Publikováno v:
Russian Journal of General Chemistry. 79:2212-2219
Reactions of 2-aryl-4-chloro-6H-1,3-thiazin-6-ones with sodium sulfide in aqueous alcohol at 18–20°C led to the formation of a readily separable mixture of 2-aryl-4-sulfanyl-6H-1,3-thiazin-6-one sodium salts (yield >70%) and bis(2-aryl-6-oxo-6H-1,
Publikováno v:
Russian Journal of Organic Chemistry. 43:1347-1356
Reactions of 1-acylthiosemicarbazides with methyl 3-phenylprop-2-ynoate provide a new one-step procedure for the synthesis of 2-substituted 5-phenyl-7H-[1,2,4]triazolo[5,1-b][1,3]thiazin-7-ones. The product structure was determined on the basis of sc
Publikováno v:
Russian Journal of Organic Chemistry. 42:783-814
The review summarizes published data on the reactions of cyclic and acyclic thioamides with derivatives of acetylenecarboxylic acids, which lead to the formation of both acyclic and heterocyclic systems, including thiazolidines and thiazines. Methods
Publikováno v:
Russian Journal of General Chemistry. 75:134-146
Readily available 5-acyl-4-hydroxy-3,6-dihydro-2H-1,3-thiazine-2,6-diones with primary alkyl- and arylamines in mild conditions (boiling in propan-2-ol) to give Schiff bases. In more rigid conditions (boiling in DMF), the reaction is accompanied by C
Publikováno v:
Russian Journal of General Chemistry. 77:155-157
Publikováno v:
Russian Journal of General Chemistry. 74:472-474
It is known that 1,3-thiazines are most commonly synthesized by reactions of thioamides, thioureas inclusive, with acetylenecarboxylic acid derivatives that play the role of a three-carbon bulding block for constructing the thiazine ring [1 4]. Accor
Publikováno v:
ChemInform. 28
Publikováno v:
ChemInform. 39
Publikováno v:
ChemInform. 34
Publikováno v:
Russian Journal of General Chemistry. 74:148-149
Condensation of thiourea with acetylenecarboxylic acid esters is well known and is used in synthesis of 1,3-thiazin-4-ones [1 4]. It is also known that N-aminothiourea (thiosemicarbazide, I) reacts with methyl propynoate in methanol to form methyl 3-