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pro vyhledávání: '"L Kacprzak"'
Autor:
Jurgen L Kacprzak, John Ziaziaris
Publikováno v:
Journal of AOAC INTERNATIONAL. 78:874-877
Samples of raw noodles in a mixture of nitric acid and hydrogen peroxide were microwave digested in sealed tetrafluoromethaxil (PTFE TFM) vessels. The digests were diluted to volume with distilled water and quantitated by inductively coupled plasma a
Autor:
J. L. Kacprzak
Publikováno v:
International Journal of Environmental Analytical Chemistry. 38:561-564
Graphite-furnace atomic absorption spectrometry for tributyltin in oysters is described. Tributyltin is extracted by n-hexane after digestion with hydrochloric acid. The 3[sgrave] detection limit for tributyltin is better than 0.01 mg Sn/kg. Typical
Autor:
J, Ziaziaris, J L, Kacprzak
Publikováno v:
Journal of AOAC International. 78(3)
Samples of raw noodles in a mixture of nitric acid and hydrogen peroxide were microwave digested in sealed tetrafluoromethaxil (PTFE TFM) vessels. The digests were diluted to volume with distilled water and quantitated by inductively coupled plasma a
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Autor:
Jurgen L Kacprzak, Ramon Chvojka
Publikováno v:
Journal of AOAC INTERNATIONAL. 59:153-157
A method for the concurrent determination of methyl mercury and inorganic mercury by flameless atomic absorption spectroscopy (AAS) is described. Fifty-seven samples of juvenile black marlin fish were analyzed for inorganic and methyl mercury, and to
Autor:
Jurgen L Kacprzak
Publikováno v:
Journal of AOAC INTERNATIONAL. 61:1528-1532
A gas-liquid chromatographic (GLC) procedure with p-toluenesulfonamide (p-TS) as an internal standard is used to determine o-toluenesulfonamide (o-TS), a major impurity in artificial sweetening substances containing saccharin. Although p-TS can itsel
Autor:
Jurgen L Kacprzak
Publikováno v:
Journal of AOAC INTERNATIONAL. 65:148-150
A method is described for determining dimethylpolysiloxane (DMPS), an antifoaming agent, in juices and beer. The method involves adsorbing the beverage onto Florisil (an activated porous magnesium silicate), drying, and Soxhlet extraction with chloro
Autor:
Jurgen L Kacprzak, Ramon Chvojka
Publikováno v:
Journal of AOAC INTERNATIONAL. 62:1179-1181
Background correction is used with a previously published flameless atomic absorption method for the concurrent determination of inorganic and methyl mercury. The use of background correction simplifies the procedure, but, more importantly, eliminate
Autor:
J L, Kacprzak
Publikováno v:
Journal - Association of Official Analytical Chemists. 61(6)
A gas-liquid chromatographic (GLC) procedure with p-toluenesulfonamide (p-TS) as an internal standard is used to determine o-toluenesulfonamide (o-TS), a major impurity in artificial sweetening substances containing saccharin. Although p-TS can itsel