Zobrazeno 1 - 10
of 28
pro vyhledávání: '"Kien-Yin Lee"'
Publikováno v:
Journal of Energetic Materials. 26:70-78
In a previous article we described the preparation and initial characterization of a novel submicron-sized HMX (sm-HMX). Using Raman spectroscopy, the sm-HMX was found to be the gamma polymorph and to be stable with respect to conversion to beta-HMX
Publikováno v:
Journal of Energetic Materials. 25:161-171
As part of our ongoing nanotechnology research effort, we have developed a novel method for the preparation of submicron-sized HMX (sm-HMX) by a simple fast-cooling technique. Surface structure analysis of the sm-HMX by field emission scanning electr
Autor:
David S. Moore, Kien-Yin Lee
Publikováno v:
Journal of Raman Spectroscopy. 38:1221-1224
Raman spectroscopy is shown to be useful as a tool for long-term stability studies. The stability of a novel submicron-size γ-polymorph form of the explosive HMX (octahydro-1,3,5,7-tetranitro-1,3,5,7-tetrazocine) was monitored up to 1 year using Ram
Autor:
Kien-Yin Lee, G. A. Buntain, Michael A. Hiskey, Betty W. Harris, Michael D. Coburn, Donald G. Ott
Publikováno v:
ChemInform. 23
Publikováno v:
ChemInform. 25
Oxidation of 3,6-diamino-1,2,4,5-tetrazine (1) with most peracids gave 3,6-diamino-1,2,4,5-tetrazine 1,4-dioxide (3) as the major product; however, treatment of (1) with peroxytrifluoroacetic acid (PTFA) gave 3,6-diamino-1,2,4,5-tetrazine 1-oxide (4)
Publikováno v:
Journal of Energetic Materials. 9:415-428
Treatment of the ammonium salt of 3,5-dinitro-1H-1,2,4-triazole (ADNT) with hydrazine hydrate gives 5-amino-3-nitro-1H-1,2,4-triazole (ANTA) in greater than 90% yields. In addition to its potential use as an insensitive high explosive, ANTA has been
Autor:
J.C. Kennedy, Kien-Yin Lee, Igor Plaksin, Adrian A Akinci, Blaine W. Asay, Jose Campos, Keith Thomas, Jose Direito, Eric S. Martin
Publikováno v:
AIP Conference Proceedings.
The floret test was originally devised to permit comparison of detonation‐spreading performance of various insensitive explosive materials, using only the dent in a copper witness plate as a metric. Dent depth in the copper plate is directly relate
Publikováno v:
Journal of Heterocyclic Chemistry. 30:1593-1595
Oxidation of 3,6-diamino-1,2,4,5-tetrazine (1) with most peracids gave 3,6-diamino-1,2,4,5-tetrazine 1,4-dioxide (3) as the major product; however, treatment of (1) with peroxytrifluoroacetic acid (PTFA) gave 3,6-diamino-1,2,4,5-tetrazine 1-oxide (4)
Publikováno v:
Acta Crystallographica Section C Crystal Structure Communications. 48:1683-1685
N 2 H 5 + .C 2 H 2 N 5 O 2 - cristallise dans Pbca avec a=5.392, b=13.316, c=18.483A, Z=8; affinement jusqu'a R=0.030. La geometrie de l'heterocycle est similaire a celle des autres 1,2,4-triazole substituees. Cette geometrie est plane dans la limite
Autor:
James E. Kennedy, Kien-Yin Lee, C. B. Skidmore, Steven F. Son, Eric S. Martin, Blaine W. Asay
Publikováno v:
AIP Conference Proceedings.
The recent discovery of significant differences in second-harmonic generation (SHG) from various grades of 1,3,5-triamino-2,4,6-trinitrobenzene (TATB) prompted an investigation into the sensitivity of TATB based upon the crystal structure and morphol