The parallel-plate resonator: An RF probe for MR and MRI studies over a wide frequency range

Autor: Andrés Ramírez Aguilera, Kevin J. Sanders, Gillian R. Goward, Bruce J. Balcom

Publikováno v: Magnetic Resonance Letters, Vol 3, Iss 4, Pp 306-318 (2023)

We explore the use of the parallel-plate resonator for the study of thin cuboid samples over a wide range of magnetic resonance frequencies. The parallel-plate resonator functions at frequencies from tens to hundreds of MHz. Seven parallel-plate reso

Externí odkaz: https://doaj.org/article/3777b2b00be44ff2a5f9a15d68c5c4fa

Multidimensional Methods and Paramagnetic NMR

Autor: Thomas Robinson, Kevin J. Sanders, Andrew J. Pell, Guido Pintacuda

Publikováno v: Two‐Dimensional (2D) NMR Methods. :415-434

Externí odkaz: https://explore.openaire.eu/search/publication?articleId=doi_________::3b0e80bcc38504288f2da6edb800342d
https://doi.org/10.1002/9781119806721.ch14

Electronic structure of Yb(III)[CH(SiMe3)2]3 from magnetic resonance spectroscopies

Autor: Anton Ashuiev, Florian Allouche, José P. Carvalho, Kevin J. Sanders, Matthew P. Conley, Daniel Klose, Giuseppe Lapadula, Michael Wörle, Dirk Baabe, Marc D. Walter, Andrew J. Pell, Christophe Copéret, Gunnar Jeschke, Guido Pintacuda, Richard A. Andersen

Characterization of paramagnetic compounds, in particular regarding the detailed conformation and electronic structure, remains a challenge - still today it often relies solely on the use of X-ray crystallography, thus limiting the access to electron

Externí odkaz: https://explore.openaire.eu/search/publication?articleId=doi_________::2ed96a1656cf9e348a88306097b27c92
https://doi.org/10.26434/chemrxiv-2023-ksfb4

Proton-detected fast-magic-angle spinning NMR of paramagnetic inorganic solids

Autor: David Proriol, Andrew J. Pell, Guido Pintacuda, Leonor Catita, Benjamin Burcher, Ladislav Benda, Kevin J. Sanders, Erwann Jeanneau, Anne-Agathe Quoineaud, Pierre-Alain Breuil, Arthur L. Lejeune, Jan Blahut

Publikováno v: RSC Advances
RSC Advances, Royal Society of Chemistry, 2021, ⟨10.1039/d1ra04110j⟩
RSC Advances, 2021, 11 (47), pp.29870-29876. ⟨10.1039/d1ra04110j⟩

International audience; Fast (60 kHz) magic angle spinning solid-state NMR allows very sensitive proton detection in highly paramagnetic organometallic powders. We showcase this technique with the complete assignment of 1 H and 13 C resonances in a h

Externí odkaz: https://explore.openaire.eu/search/publication?articleId=doi_dedup___::dfe07a75e72d76ea68f8ac5f4686c5f6
https://hal.archives-ouvertes.fr/hal-03454812/file/RSCAdv.pdf

Picometer Resolution Structure of the Coordination Sphere in the Metal-Binding Site in a Metalloprotein by NMR

Autor: Isabella C. Felli, Andrea Bertarello, Leonardo Gonnelli, Kevin J. Sanders, Michael John Knight, Martin Kaupp, Lyndon Emsley, G. Pintacuda, Roberta Pierattelli, Vladimir Pelmenschikov, Andrew J. Pell, Ladislav Benda

Publikováno v: Journal of the American Chemical Society
Journal of the American Chemical Society, 2020, 142 (39), pp.16757-16765. ⟨10.1021/jacs.0c07339⟩
Journal of the American Chemical Society, American Chemical Society, 2020, 142 (39), pp.16757-16765. ⟨10.1021/jacs.0c07339⟩

Most of our understanding of chemistry derives from atomic-level structures obtained with single-crystal X-ray diffraction. Metal centers in X-ray structures of small organometallic or coordination complexes are often extremely well-defined, with err

Externí odkaz: https://explore.openaire.eu/search/publication?articleId=doi_dedup___::4685a45d0cd3e1812df621d6ed53cc66
https://pubmed.ncbi.nlm.nih.gov/32871082