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Publikováno v:
Zeitschrift für Naturforschung B. 49:1361-1367
A simple route to 1,3-diphosphetanes [RPCF2]2 [R = Ph, Me, But] is described. The phosphaalkene intermediates RP=CF2, as well as the corresponding disulfides [R(S)PCF2]2 have been characterized. The crystal structures of [PhPCF2]2, and of the sulfide