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of 6
pro vyhledávání: '"Jun Fukazawa"'
Autor:
Marek Pruski, Jun Fukazawa, Frédéric A. Perras, Takeshi Kobayashi, Yoh Matsuki, Toshimichi Fujiwara
Publikováno v:
Physical Chemistry Chemical Physics. 23:4919-4926
Despite the growing number of successful applications of dynamic nuclear polarization (DNP)-enhanced magic-angle spinning (MAS) NMR in structural biology and materials science, the nuclear polarizations achieved by current MAS DNP instrumentation are
Publikováno v:
Journal of the American Chemical Society. 132:4290-4294
To establish a relationship between the secondary structure of a peptide and the quadrupolar coupling of its amide (14)N, we examined (14)N quadrupolar couplings for eight different polypeptide samples, each of whose secondary structure (alpha-helix
Publikováno v:
Journal of magnetic resonance (San Diego, Calif. : 1997). 264
Sensitivity enhancement of MAS NMR using dynamic nuclear polarization (DNP) is gaining importance at moderate fields (B090K) with potential applications in chemistry and material sciences. However, considering the ever-increasing size and complexity
Publikováno v:
Journal of magnetic resonance (San Diego, Calif. : 1997). 211(1)
In this work, we examine the fluctuation of the intensity and the phase of an NMR signal during repetition of experiments and investigate possibilities of using these information to judge suspicious peaks, whose true colors may be noises or genuine s
Autor:
Jun Fukazawa, Kiyonori Takegoshi
Publikováno v:
Physical Chemistry Chemical Physics. 12:11225
To examine noisy nuclear-magnetic resonance (NMR) spectra, we have developed a novel signal analysis method based on phase correlation between the NMR signal and the excitation pulse. The new phase-covariance analysis is compatible with the conventio
Publikováno v:
Journal of the Physical Society of Japan. 77:044711
11 B nuclear magnetic resonance (NMR) measurements have been performed on MgB 2 powder sample at several magnetic fields ranging from 6.3 to 21.9 T. The isotropic Knight-shift, as well as quadrupole coupling frequency, was accurately determined from