Zobrazeno 1 - 10
of 55
pro vyhledávání: '"Josef Novosad"'
Publikováno v:
Polyhedron. 124:62-67
New reaction systems leading to cadmium, mercury and lead selenides and tellurides are reported. The chalcogenides were prepared by a simple, direct reaction between chalcogen, metal oxide or carbonate, and 3-(diphenylphosphino)propionic acid. The sy
Autor:
Václav Kubát, Zdeněk Trávníček, Lukáš Jeremias, Michal Babiak, Josef Novosad, Maria José Calhorda
Publikováno v:
Inorganica Chimica Acta. 443:230-234
The oxidation of Ph2P(CH2)(n)PPh2 (n = 1, 3, 5) by tellurium powder was studied. The prepared compounds Ph2P(Te)(CH2)(n)P(Te)Ph-2 (1, n = 3; 2, n = 5) were characterized by P-31 and Te-125 NMR spectroscopy, elemental analysis, FTIR spectroscopy and f
Publikováno v:
Phosphorus, Sulfur, and Silicon and the Related Elements. 189:1475-1488
A series of zinc(II) and cadmium(II) complexes, involving a combination of S-donor (xanthates and dithiophosphates) and N-donor (1,10-phen = 1,10-phenanthroline, 2,2-bipy = 2,2-bipyridine) ligands, of the composition [Cd(S2COnPr)2(2,2-bipy)] (1), [Cd
Publikováno v:
Zeitschrift für Kristallographie - Crystalline Materials. 229:537-542
The detailed X-ray structural elucidation of reaction products of a zinc(II) salt with O,O′-dialkyldithiophosphate and nitrogen-containing heterocycles (N–N=1,10-phenanthroline (phen) or 2,2′-bipyridine (bpy)) has been performed. Surprisingly,
Publikováno v:
Phosphorus Research Bulletin. 19:48-53
Publikováno v:
Phosphorus Research Bulletin. 19:30-35
Publikováno v:
Phosphorus Research Bulletin. 19:83-89
Publikováno v:
Inorganic Chemistry Communications. 38:8-10
A new method of synthesis for the formation of metal tellurides of the type MTe (M=Cd, Hg) is reported. The compounds were prepared by the reaction of cadmium carbonate (or mercury oxide, respectively) with tellurium and bis(diphenylphosphino)amine i
Publikováno v:
Inorganica Chimica Acta. 356:319-327
Te(II) forms binuclear complexes with bridging [{S=P(Ph)(2)}(2)N](-) ligands and axial aryl groups with very long (TeTe)-Te-... distances, while Te(I) analogues with [S2P(R)(2)](-) have no axial ligands and exhibit a Te-Te bond. No such selenium comp
Publikováno v:
Polyhedron. 22:1585-1593
The synthesis and spectroscopic characterization of three chalcogenophosphoryl ligands derived from pyridine is reported. The synthesis was based on the oxidation of C5H3N(PPh2)(2) by elemental sulfur and selenium, and hydrogen peroxide. As a part of