Zobrazeno 1 - 10
of 52
pro vyhledávání: '"John J. Langenfeld"'
Publikováno v:
Journal of Chromatography A. 740:139-145
Desorption profiles of analytes using a conventional split/splitless injection port after solid-phase microextraction were determined in real-time by direct coupling of the injection port to a mass spectrometer. Desorption times for aromatic hydrocar
Publikováno v:
Analytical Chemistry. 67:1727-1736
Supercritical fluid extraction (SFE) rates of spiked polychlorinated dibenzo-p-dioxins (PCDDs) from Florisil, spiked [ 13 C]PCDDs and native PCDDs from fly ash, and spiked [ 2 H]polycyclic aromatic hydrocarbons (PAHs) and native PAHs from marine sedi
Publikováno v:
Analytical Chemistry. 66:909-916
Supercritical fluid extraction (SFE) using eight different CO[sub 2] + organic modifier mixtures and one ternary mixture (CO[sub 2] + methanol/toluene) at two different concentrations (1 and 10% v/v) was performed on two certified reference materials
Publikováno v:
Analytical chemistry. 68(1)
Solid-phase microextraction (SPME) parameters were examined on water contaminated with hydrocarbons including benzene and alkylbenzenes, n-alkanes, and polycyclic aromatic hydrocarbons (PAHs). Absorption equilibration times ranged from several minute
Autor:
Peter K.K. Louie, Mark D. Burford, Steven B. Hawthorne, David J. Miller, John J. Langenfeld, Sally E. Eckert-Tilotta
Publikováno v:
Journal of Chromatography A. 642:301-317
The development of quantitative supercritical fluid extraction (SFE) methods for the recovery of organic pollutants from environmental samples requires three steps: quantitative partitioning of the analytes from the sample into the extraction fluid,
Publikováno v:
Analytical Chemistry. 65:338-344
Three certified reference materials, polychlorinated biphenyls (PCBs) from river sediment, polycyclic aromatic hydrocarbons (PAHs) from urban air particulate matter, and PAHs from highly contaminated soil, were extracted with pure CO[sub 2] at conven
Publikováno v:
Environmental Science & Technology. 26:2251-2262
Organic pollutants from winter urban air were collected using a conventional PM-10 high-volume air sampler (68 m 3 /h) which had been modified to include polyyrethane foam (PUF) sorbent sheets behind the quartz fiber filter. Fifty-five major semivola
Publikováno v:
Analytical Chemistry. 64:2263-2266
Densities of three pure supercritical fluids (Co 2 , N 2 O, and CHCIF 2 ) and one modified fluid (Co 2 modified with 5 volume % methanol) were determined over a wide range of pressures (60-600 atm) and temperatures (40-150 o C) using a simple device
Publikováno v:
Analytical Chemistry. 64:1614-1622
Supercritical fluid extraction (SFE) recoveries for native pollutants including PCBs from a standard reference material sediment (SRM 1939), PAHs from a petroleum waste sludge, and PAHs from railroad bed soil were compared using supercritical CHCIF 2
Publikováno v:
Journal of Chromatography A. 594:297-307
Supercritical fluid extraction (SFE) collection efficiences of 66 compounds with a wide range of volatility and polarity were examined. Good collection efficiencies required efficient partitioning of the analyte into the collection solvent after depr