Zobrazeno 1 - 10
of 18
pro vyhledávání: '"John J. Balbach"'
Publikováno v:
Biophysical Journal. 86:428-434
Solid-state NMR measurements have been reported for four peptides derived from beta-amyloid peptide Abeta(1-42): Abeta(1-40), Abeta(10-35), Abeta(16-22), and Abeta(34-42). Of these, the first two are predicted to be amphiphilic and were reported to f
Publikováno v:
Chemical Physics. 266:231-236
A two-dimensional solid state NMR technique for measurements of dipole–dipole couplings in many-spin systems under high-speed magic-angle spinning (MAS) is described. The technique, called constant-time finite-pulse radio-frequency-driven recouplin
Publikováno v:
Chemistry of Materials. 12:973-982
Nanocrystalline nickel aluminides (nano-NiAl and nano-Ni3Al) are synthesized by reactions of NiCl2 and LiAlH4 in Et2O or 1,3,5-trimethylbenzene, followed by annealing of the reaction products at 55...
Autor:
John J. Balbach, Vitali Tugarinov, Jacob Anglister, Peter J. Steinbach, David P. Weliky, Jun Yang, Robert Tycko
Publikováno v:
Journal of Biomolecular NMR. 16:313-327
We describe solid state NMR measurements on frozen solutions of the complex of the 24-residue HIV-1 gp120 V3 loop peptide RP135 with the Fab fragment of the anti-gp120 antibody 0.5β, using rotational echo double resonance (REDOR). In order to probe
Publikováno v:
Physical Review B. 60:966-971
Nuclear magnetic resonance measurements of the {sup 45}Sc, {sup 1}H, and {sup 2}D spin-lattice relaxation rates in the solid solutions {alpha}-ScH{sub x} (x=0, 0.11, and 0.27) and {alpha}-ScD{sub x} (x=0.05 and 0.22) have been performed over the temp
Publikováno v:
Physical Review B. 59:3769-3774
Publikováno v:
Physical Review B. 58:14823-14832
Three samples of ${\mathrm{YD}}_{x},$ with x ranging from 2.9 to nearly 3.0, were studied with deuterium nuclear magnetic resonance to gain insight into the locations of the D atoms in the lattice and their motions. Line shapes at low temperatures (2
Autor:
John J. Balbach, Mark S. Conradi, David P. Cistola, Changguo Tang, Joel R. Garbow, William C. Hutton
Publikováno v:
Chemical Physics Letters. 277:367-374
A new NMR technique is presented that yields high-resolution, 1-D NMR spectra of solutes in inhomogeneous magnetic fields. The method exploits the nuclear Overhauser effect which couples the longitudinal relaxation of solvent and solute nuclear spins
Publikováno v:
Physical Review B. 53:15054-15062
Magic-angle-spinning ~MAS! deuterium NMR of YD x , x;2, yields spectrally resolved lines for D atoms in tetrahedral (T) and octahedral (O) interstitial sites. Compared to MAS line narrowing of metal hydrides, the deuterides line narrow with only mode
Autor:
Mark S. Conradi, Johanna L. Crane, John J. Balbach, William E. Buhro, Claire A. Frey, Joel A. Haber, S.M.L. Sastry
Publikováno v:
Advanced Materials. 8:163-166