Zobrazeno 1 - 10
of 12
pro vyhledávání: '"Joerg Daniels"'
Publikováno v:
Angewandte Chemie International Edition. 55:1173-1177
As a new method for the synthesis of chalcogen polycationic clusters, the electrochemical dissolution of elemental tellurium in ionic liquids (IL) or in liquid SO2 is presented. ILs used are ethylmethylimidazolium triflate [OTf](-) and tetraalkylammo
Autor:
Gregor Schnakenburg, Joerg Daniels, Andreas Eich, Wilfried Hoffbauer, Thomas Bredow, Johannes Beck
Publikováno v:
European Journal of Inorganic Chemistry. 2014:3043-3052
The reactions of elemental antimony, tellurium, selenium and sulfur as well as antimony telluride and antimony sulfide in melts composed of GaCl3/SbCl3/ACl (A = Cu+, Ag+, PPh4+) yielded Ag(Sb7Te8)[GaCl4]6 (1), (Sb7Se8)[GaCl4]2[Ga2Cl7]3 (2), (Sb7Se8Cl
Publikováno v:
Zeitschrift für anorganische und allgemeine Chemie. 639:2463-2472
ReVIIO2(PO4) and (ReVII2O5)Sio2[Sit2O(PO4)6] were obtained from Re2O7 and P4O10 in sealed silica tubes (250 ≤ ϑ ≤ 400 °C). The crystal structures were solved and refined from X-ray single crystal data (ReVIIO2(PO4): C2/c, Z = 24, a = 14.403(1)
Publikováno v:
ChemInform. 47
As a new method for the synthesis of chalcogen polycationic clusters, the electrochemical dissolution of elemental tellurium in ionic liquids (IL) or in liquid SO2 is presented. ILs used are ethylmethylimidazolium triflate [OTf](-) and tetraalkylammo
Publikováno v:
Zeitschrift für anorganische und allgemeine Chemie. 638:1820-1826
The reaction of metallic bismuth with either tungsten tetrachlorideoxide WOCl4 at 650 K or tungsten tetrabromideoxide WOBr4 at 670 K, respectively, leads to BiX2[W2O2X6] (X = Cl, Br) as black, lustrous crystal needles. The crystal structure determina
Autor:
Joerg Daniels, Johannes Beck, Wilfried Hoffbauer, Andreas Eich, Thomas Bredow, Gregor Schnakenburg
Publikováno v:
ChemInform. 45
The compounds (VI), (VIII), (IX), and (XI), which form orange, air-sensitive crystals are characterized by single crystal XRD, X-ray fluorescence spectroscopy, Raman spectroscopy, solid state 77Se NMR spectroscopy, and DFT calculations.
Publikováno v:
ChemInform. 45
ReVIIO2(PO4) (I) and (ReVII2O5)Si2 [Si2O(PO4)6] (II) are obtained from the reaction of Re2O7 and P4O10 in sealed silica tubes (temperature gradient 400 300 °C, 2 d).
Publikováno v:
ChemInform. 43
BiCl2[W2O2Cl6] is prepared by reaction of metallic Bi and WOCl4 (sealed silica tube, 650 K, 7 d; 80% yield) and BiBr2[W2O2Br6] is obtained from Bi and WOBr4 (670 K, 50 d; 20% yield).
Autor:
Anna Isaeva, Joerg Daniels, Andreas Heerwig, Ejaz Ahmed, Alexander Stankowski, Walter Schnelle, Sven Lidin, Thomas Doert, Michael Ruck, Steffen Jan Eck, Johannes Beck
Publikováno v:
Angewandte Chemie (International ed. in English). 51(32)
Publikováno v:
ChemInform. 42