Zobrazeno 1 - 5
of 5
pro vyhledávání: '"Jihchin Chung"'
Autor:
Reginald O. Cann, Matthew Richard Oberholzer, Robert E. Waltermire, Jiri Kasparec, Yun K. Ye, Jihchin Chung, Robert Wethman
Publikováno v:
Organic Process Research & Development. 14:1147-1152
Two efficient large scale syntheses of (Z)-(1-bromobut-1-ene-1,2-diyl)dibenzene are described. The first is a three-step synthetic sequence from trimethyl(phenylethynyl)silane in 63% overall yield. The key transformations involved the stereospecific
Publikováno v:
Synthetic Communications. 29:3811-3820
High yields of several thiolesters of 2-[3-(4-cyanophenyl)-4,5-dihydro-5-isoxazolyl]acetic acid are easily prepared from the corresponding oxoester by the reaction with trimethyl silylated mercaptan and aluminum chloride. The selection of mercaptans
Publikováno v:
ChemInform. 28
A convergent, large-scale, chiral synthesis of isoxazoline 1 has been achieved in 37% overall yield and >99.6% optical purity, starting from l-asparagine and 4-cyanobenzaldehyde. Hofmann reaction of Nα-n-Boc-l-asparagine with iodosobenzene diacetate
Publikováno v:
ChemInform. 31
High yields of several thiolesters of 2-[3-(4-cyanophenyl)-4,5-dihydro-5-isoxazolyl]acetic acid are easily prepared from the corresponding oxoester by the reaction with trimethyl silylated mercaptan and aluminum chloride. The selection of mercaptans
Publikováno v:
The Journal of organic chemistry. 62(8)
A convergent, large-scale, chiral synthesis of isoxazoline 1 has been achieved in 37% overall yield and99.6% optical purity, starting from L-asparagine and 4-cyanobenzaldehyde. Hofmann reaction of N(alpha)-n-Boc-L-asparagine with iodosobenzene diacet