Zobrazeno 1 - 10
of 37
pro vyhledávání: '"Jeffrey M. Manthorpe"'
Publikováno v:
SynOpen, Vol 02, Iss 02, Pp 0168-0175 (2018)
Abstract The total synthesis of isotopically labelled (9R,10S)-dihydrosterculic acid, a usual cyclopropane fatty acid with biologically relevant toxicity upon desaturation in vivo, is reported. A diastereoselective Corey–Chaykovsky reaction was
Externí odkaz:
https://doaj.org/article/2d3c7bfe259b46c889a94febc691f7ac
Publikováno v:
Sensors, Vol 16, Iss 10, p 1697 (2016)
Bisphenol A (BPA) is an estrogen-mimicking chemical that can be selectively detected in water using a chemical sensor based on molecularly imprinted polymers (MIPs). However, the utility of BPA-MIPs in sensor applications is limited by the presence o
Externí odkaz:
https://doaj.org/article/436f2358697147a19e84b63c5e9f246e
Autor:
Christian A. Rosales, Samuel W. J. Shields, Chelsey L. J. Aulenback, Gazmend Elezi, Karl V. Wasslen, Peter J. Pallister, Kym F. Faull, Jeffrey M. Manthorpe, Jeffrey C. Smith
Publikováno v:
Journal of the American Society for Mass Spectrometry. 34:948-957
Autor:
Jeffrey M. Manthorpe, Jonathan Day, Volodymyr Semeniuchenko, Sepideh Sharif, William J. Pietro, Michael G. Organ, Nalin Chandrasoma, Wilfried M. Braje
Publikováno v:
The Journal of Organic Chemistry. 86:10343-10359
(DiMeIHeptCl)Pd, a hyper-branched N-aryl Pd NHC catalyst, has been shown to be efficient at performing amine arylation reactions in solvent-free ("melt") conditions. The highly lipophilic environment of the alkyl chains flanking the Pd center serves
Autor:
Debasis Mallik, Jeffrey M. Manthorpe, Wenyao Zhang, Mathieu A. Morin, William J. Pietro, Michael G. Organ
Publikováno v:
Chemistry–Methods. 1:131-134
Autor:
Scott A. McLuckey, Jeffrey C. Smith, Elissia T. Franklin, Jeffrey M. Manthorpe, Samuel W. J. Shields, Yu Xia
Publikováno v:
J Am Soc Mass Spectrom
Shotgun lipidomics provides sensitive and fast lipid identification without the need for chromatographic separation. Challenges faced by shotgun analysis of glycerophospholipids (GPs) include the lack of signal uniformity across GP classes and the in
Autor:
Christian A. Rosales, Joshua A. Roberts, Jeffrey C. Smith, Samuel W. J. Shields, Peter J. Pallister, Jeffrey M. Manthorpe, Karl V. Wasslen
Publikováno v:
Analytical chemistry. 93(2)
Trimethylation enhancement using diazomethane (TrEnDi) is a derivatization technique that significantly enhances the signal intensity of glycerophospholipid species in mass spectrometry (MS) and tandem mass spectrometry (MS/MS) analyses. Here, we des
Autor:
Stella K. Betancourt, Scott A. McLuckey, Jeffrey M. Manthorpe, Carlos R. Canez, Jeffrey C. Smith, Samuel W. J. Shields
Publikováno v:
Analytical Chemistry. 89:9452-9458
Methylation of phospholipids (PL) leads to increased uniformity in positive electrospray ionization (ESI) efficiencies across the various PL subclasses. This effect is realized in the approach referred to as “trimethylation enhancement using 13C-di
Autor:
Magdalena Bugno, Hillary P. Weinert, Jeffrey M. Manthorpe, Karl V. Wasslen, William G. Willmore, Jeffrey C. Smith, Carlos R. Canez, Samuel W. J. Shields
Publikováno v:
Analytical Chemistry. 88:6996-7004
Significant sensitivity enhancements in the tandem mass spectrometry-based analysis of complex mixtures of several phospholipid classes has been achieved via (13)C-TrEnDi. (13)C-TrEnDi-modified phosphatidylethanolamine (PE), phosphatidylserine (PS),
Publikováno v:
Food Control. 50:778-783
Bisphenol A (BPA) is an endocrine disrupting compound commonly found in consumer plastic goods. For environmental and food analyses, however, selective extraction of BPA in the presence of other organic compounds will be challenging unless a molecula