Zobrazeno 1 - 10
of 10
pro vyhledávání: '"Jared, Nieboer"'
Autor:
Michael Gerken, Xin Yu, Jared Nieboer, Hélène P. A. Mercier, Ralf Haiges, William Hillary, Tyler Richardet
Publikováno v:
Inorganic Chemistry. 51:6350-6359
The new [N(CH3)4][WSF5] salt was synthesized by two preparative methods: (a) by reaction of WSF4 with [N(CH3)4][F] in CH3CN and (b) directly from WF6 using the new sulfide-transfer reagent [N(CH3)4][SSi(CH3)3]. The [N(CH3)4][WSF5] salt was characteri
Publikováno v:
Zeitschrift für anorganische und allgemeine Chemie. 638:520-525
The new Lewis-acid-base adduct of WSF4 and pyridine, WSF4·NC5H5, was prepared by combination of WSF4 and excess pyridine. The WSF4·NC5H5 adduct was characterized by 1H, 13C, 19F NMR, and Raman spectroscopy, and by X-ray crystallography. Calculation
Publikováno v:
Inorganic Chemistry. 48:11251-11258
A new and improved synthetic route to WSF(4) was developed from the reaction of WF(6) and Sb(2)S(3) in anhydrous HF. Tungsten sulfide tetrafluoride was characterized by Raman and (19)F NMR spectroscopy for the first time in HF solvent. Both studies p
Publikováno v:
Journal of Fluorine Chemistry. 125:1163-1168
The xenon fluorides, XeF2, XeF4, and XeF6, were characterized by gas-phase 129 Xe and 19 F NMR spectroscopy, providing the first gas-phase NMR spectroscopic data for the xenon fluorides. Xenon difluoride was also characterized in the solid state by s
Autor:
Helen P. A. Mercier, Michael Gerken, Xin Yu, Tyler Richardet, Ralf Haiges, Jared Nieboer, William Hillary
Publikováno v:
ChemInform. 43
The new compound (III) is synthesized by reaction of (I) and (II) (yield given in g) and directly from (IV) using the new sulfide-transfer reagent (V).
Autor:
Jared, Nieboer, Ralf, Haiges, William, Hillary, Xin, Yu, Tyler, Richardet, Hélène P A, Mercier, Michael, Gerken
Publikováno v:
Inorganic chemistry. 51(11)
The new [N(CH(3))(4)][WSF(5)] salt was synthesized by two preparative methods: (a) by reaction of WSF(4) with [N(CH(3))(4)][F] in CH(3)CN and (b) directly from WF(6) using the new sulfide-transfer reagent [N(CH(3))(4)][SSi(CH(3))(3)]. The [N(CH(3))(4
Publikováno v:
Inorganic chemistry. 49(13)
Molybdenum sulfide tetrafluoride was synthesized from MoF(6) and S(Si(CH(3))(3))(2) in CFCl(3) at low temperature and was fully characterized by Raman, infrared, and (19)F NMR spectroscopy and by X-ray crystallography. The crystal structure revealed
Publikováno v:
ChemInform. 41
A new and improved synthetic route to WSF4 was developed from the reaction of WF6 and Sb2S3 in anhydrous HF. Tungsten sulfide tetrafluoride was characterized by Raman and 19F NMR spectroscopy for t...
Autor:
Jared Nieboer, Paul Hazendonk, Adriana Iuga, Evgeny Goreshnik, Melita Tramsek, Shaohui Zheng, Michael Gerken, Boris Zemva, Jochen Autschbach
Publikováno v:
Inorganic chemistry. 46(15)
The coordination compounds [Mg(XeF(2))(2)][AsF(6)](2), [Mg(XeF(2))(4)][AsF(6)](2), [Ca(XeF(2))(2.5)][AsF(6)](2), [Ba(XeF(2))(3)][AsF(6)](2), and [Ba(XeF(2))(5)][AsF(60](2) were characterized by solid-state (19)F and (129)Xe magic-angle spinning NMR s
Publikováno v:
ChemInform. 35