Zobrazeno 1 - 7
of 7
pro vyhledávání: '"Jan Paulson"'
Publikováno v:
Journal of Neurochemistry. 62:2030-2036
Model melanins, synthesized with different cysteinyldopamine/dopamine ratios in the incubates, were oxidized with KMnO4 and the resulting compounds were analyzed by HPLC. The ratios between a phaeomelanin-derived compound, thiazole-4,5-dicarboxylic a
Publikováno v:
Biological Mass Spectrometry. 21:525-533
(22R,S)Budesonide was isolated from human plasma by solid-phase extraction. Switching from reversed-phase conditions during sample application and washing to normal-phase conditions during elution afforded a very clean extract. Budesonide was derivat
Publikováno v:
Journal of Chromatography A. 554:215-226
An automated thermospray liquid chromatography-mass spectrometry system is described, including an autosampler and a gradient liquid chromatography system controlled from the mass spectrometer data system. The performance and reliability of the equip
Publikováno v:
Biological Mass Spectrometry. 19:218-224
(R,S)-Bambuterol was isolated from plasma and urine by solid-phase extraction and analysed as its trimethylsilyl derivative by gas chromatography/chemical ionization mass spectrometry with ammonia as the reagent gas. Deuterium-labelled bambuterol was
Autor:
Jan Paulson, Claes Lindberg
Publikováno v:
Journal of chromatography. 554(1-2)
The 21-hydroxyl group of cortisol was selectively acetylated under mild conditions without affecting the more sterically hindered 11 beta- and 17 alpha-hydroxyl groups. The reaction was performed with a mixture of acetic anhydride and triethylamine i
Publikováno v:
Biological Mass Spectrometry. 14:535-541
A moving belt interface was used to identify budesonide metabolites, obtained from rat and mouse liver incubations, by liquid chromatography/mass spectrometry (LC/MS). The metabolites were separated on a small-bore C18 column with an ethanol/water gr
Autor:
Claes Lindberg, Jan Paulson
Publikováno v:
Journal of Chromatography A. 394:117-122
Vaporizer temperature and repeller potential were optimized for five test compounds analysed by liquid chromatography—thermospray mass spectrometry. Optimum values were about the same for most compounds. The MH + ion intensity of one thermally labi