Zobrazeno 1 - 10
of 12
pro vyhledávání: '"James J. Weeks"'
Autor:
Peter K, Sullivan, James J, Weeks
Publikováno v:
J Res Natl Bur Stand A Phys Chem
The diffraction of x-rays by the crystalline n-paraffins, C(36)H(74), C(44)H(90), and C(94)H(190), was examined at small angles – below seven degrees 2θ – as a function of temperature. The Bragg maxima (00l) that occur at these angles result fro
Autor:
Norman Bekkedahl, James J. Weeks
Publikováno v:
Journal of research of the National Bureau of Standards. Section A, Physics and chemistry. (2)
An adiabatic copper calorimeter was used to determine the heats of vulcanization of pale crepe natural rubber with sulfur for mixtures varying in composition from 0 to 32 per cent added sulfur. The side reaction that produces hydrogen sulfide was avo
Autor:
James J. Weeks
Publikováno v:
Journal of Research of the National Bureau of Standards. Section A, Physics and Chemistry
The melting temperature of linear polyethylene has been obtained as a function of the time and temperature of crystallization. Recrystallization was minimized by a special melting procedure. By interpreting the melting points as characteristic of a g
Publikováno v:
Journal of Research of the National Bureau of Standards. Section A, Physics and Chemistry
The rate of isothermal bulk crystallization of poly(chlorotrifluoroethylene), Tm =221° C, was measured from 170° to 200° C. The intrinsic bulk crystallization, which accurately followed an n = 2 law, was shown to be a result of the injection of pr
Autor:
Shu-Sing Chang, James J. Weeks
Publikováno v:
Journal of Research of the National Institute of Standards and Technology
Heat capacities and thermodynamic properties of a number of poly(chlorotrifluoToethylene) samples subjected to various thermal treatments, to achieve crystallinities ranging from approximately 10 to 90%, have been studied from 2.5 to 370 K by automat
Autor:
John D. Hoffman, James J. Weeks
Publikováno v:
Journal of Polymer Science. 28:472-475
Autor:
John D. Hoffman, James J. Weeks
Publikováno v:
The Journal of Chemical Physics. 37:1723-1741
(I) The requirements for making a critical test of whether two‐ or three‐dimensional surface nucleation controls the radial growth of lamellar spherulites in bulk are discussed. Radial‐growth‐rate data were obtained on spherulites of polychlo
Autor:
John D. Hoffman, James J. Weeks
Publikováno v:
The Journal of Chemical Physics. 42:4301-4302
Autor:
Peter K. Sullivan, James J. Weeks
Publikováno v:
Journal of Research of the National Bureau of Standards Section A: Physics and Chemistry. :203
The diffraction of x-rays by the crystalline n-paraffins, C36H74, C44H90, and C94H190, was examined at small angles - below seven degrees 2θ - as a function of temperature. The Bragg maxima (00l) that occur at these angles result from a lamellar rep
Autor:
James J. Weeks, John D. Hoffman
Publikováno v:
Journal of Research of the National Bureau of Standards Section A: Physics and Chemistry. :13
A new method of estimating the equilibrium melting temperature, Tm, of a polymer is described, and applied to polychlorotrifluoroethylene (PCTFE). Experimentally determined values of the so-called observed melting point, !F^(obs), are plotted as a fu